tert-Butyl 5-(6-(3-(benzyloxy)phenylthio)-1,2,3,4-tetrahydronaphthalen-2-yl)-2,2-dimethyl-1,3-dioxan-5-ylcarbamate

Base Information

Chemical Name:tert-Butyl 5-(6-(3-(benzyloxy)phenylthio)-1,2,3,4-tetrahydronaphthalen-2-yl)-2,2-dimethyl-1,3-dioxan-5-ylcarbamate
CAS No.:1225230-11-4
Molecular Formula:C₃₄H₄₁NO₅S
Molecular Weight:575.769
Hs Code.:

Synonyms:tert-Butyl 5-(6-(3-(benzyloxy)phenylthio)-1,2,3,4-tetrahydronaphthalen-2-yl)-2,2-dimethyl-1,3-dioxan-5-ylcarbamate

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Chemical Property of tert-Butyl 5-(6-(3-(benzyloxy)phenylthio)-1,2,3,4-tetrahydronaphthalen-2-yl)-2,2-dimethyl-1,3-dioxan-5-ylcarbamate

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Technology Process of tert-Butyl 5-(6-(3-(benzyloxy)phenylthio)-1,2,3,4-tetrahydronaphthalen-2-yl)-2,2-dimethyl-1,3-dioxan-5-ylcarbamate

There total 5 articles about tert-Butyl 5-(6-(3-(benzyloxy)phenylthio)-1,2,3,4-tetrahydronaphthalen-2-yl)-2,2-dimethyl-1,3-dioxan-5-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 431878-96-5
3-(benzyloxy)benzenethiol

: 1225230-10-3
6-(5-(tert-Butoxycarbonylamino)-2,2-dimethyl-1,3-dioxan-5-yl)-5,6,7,8-tetrahydronaphthalen-2-yl trifluoromethanesulfonate

: 1225230-11-4
tert-Butyl 5-(6-(3-(benzyloxy)phenylthio)-1,2,3,4-tetrahydronaphthalen-2-yl)-2,2-dimethyl-1,3-dioxan-5-ylcarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In 1,4-dioxane; Inert atmosphere of nitrogen; Heating; Reflux;

Reference yield:

: 1225230-05-6
2-(Benzylamino)-2-(6-(benzyloxy)-3,4-dihydronaphthalen-2-yl)propane-1,3-diol

: 1225230-11-4
tert-Butyl 5-(6-(3-(benzyloxy)phenylthio)-1,2,3,4-tetrahydronaphthalen-2-yl)-2,2-dimethyl-1,3-dioxan-5-ylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid; Pd-C / ethyl acetate; ethanol

2: sodium hydrogencarbonate / methanol; tetrahydrofuran; water; diethyl ether

3: sodium hydrogencarbonate; trifluoroborane diethyl ether; p-toluenesulfonic acid monohydrate / methanol; ethyl acetate

4: dichloromethane

5: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; Pd-C; p-toluenesulfonic acid monohydrate; trifluoroborane diethyl ether; sodium hydrogencarbonate; acetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; ethanol; dichloromethane; water; ethyl acetate;

Reference yield:

: 1225230-07-8
2-Amino-2-(6-hydroxy-1,2,3,4-tetrahydronaphthalen-2-yl)propane-1,3-diol

: 1225230-11-4
tert-Butyl 5-(6-(3-(benzyloxy)phenylthio)-1,2,3,4-tetrahydronaphthalen-2-yl)-2,2-dimethyl-1,3-dioxan-5-ylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / methanol; tetrahydrofuran; water; diethyl ether

2: sodium hydrogencarbonate; trifluoroborane diethyl ether; p-toluenesulfonic acid monohydrate / methanol; ethyl acetate

3: dichloromethane

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; p-toluenesulfonic acid monohydrate; trifluoroborane diethyl ether; sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane; water; ethyl acetate;