3-methoxycarbonyl-9-methyl-1-phenyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

Base Information

Chemical Name:3-methoxycarbonyl-9-methyl-1-phenyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide
CAS No.:93598-49-3
Molecular Formula:C₂₀H₁₈N₂O₂*HI
Molecular Weight:446.288
Hs Code.:

Synonyms:3-methoxycarbonyl-9-methyl-1-phenyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methoxycarbonyl-9-methyl-1-phenyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

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Technology Process of 3-methoxycarbonyl-9-methyl-1-phenyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

There total 2 articles about 3-methoxycarbonyl-9-methyl-1-phenyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 93598-52-8
N^α-phenylthiocarbonyl-1-methyltryptophan methyl ester

: 93598-49-3
3-methoxycarbonyl-9-methyl-1-phenyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

Guidance literature:: With methyl iodide; In acetonitrile; at 50 ℃; for 96h;
DOI:10.1248/cpb.33.3237

Reference yield:

: 104331-10-4
2-Benzoylamino-3-(1-methyl-1H-indol-3-yl)-propionic acid methyl ester

: 93598-49-3
3-methoxycarbonyl-9-methyl-1-phenyl-3,4-dihydro-9H-pyrido<3,4-b>indole hydriodide

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Lawesson's reagent / 1,2-dimethoxy-ethane / 3 h / Ambient temperature

2: 79 percent / CH₃I / acetonitrile / 96 h / 50 °C

With Lawessons reagent; methyl iodide; In 1,2-dimethoxyethane; acetonitrile;
DOI:10.1248/cpb.33.3237