[Fe(5⁽²⁾-N-(4-aza-18-crown-6)methyl-5⁽⁴⁾,10⁽⁴⁾,15⁽⁴⁾,20⁽⁴⁾-tetra-tert-butyl-5⁽⁶⁾-methyl-5,10,15,20-tetraphenylporphyrin-2H)2O]

Base Information

• Chemical Name: [Fe(5⁽²⁾-N-(4-aza-18-crown-6)methyl-5⁽⁴⁾,10⁽⁴⁾,15⁽⁴⁾,20⁽⁴⁾-tetra-tert-butyl-5⁽⁶⁾-methyl-5,10,15,20-tetraphenylporphyrin-2H)2O]
• CAS No.: 936131-20-3
• Molecular Formula: C₁₄₈H₁₇₄Fe₂N₁₀O₁₁
• Molecular Weight: 2380.76

Synonyms:[Fe(5⁽²⁾-N-(4-aza-18-crown-6)methyl-5⁽⁴⁾,10⁽⁴⁾,15⁽⁴⁾,20⁽⁴⁾-tetra-tert-butyl-5⁽⁶⁾-methyl-5,10,15,20-tetraphenylporphyrin-2H)2O]

Chemical Property of [Fe(5⁽²⁾-N-(4-aza-18-crown-6)methyl-5⁽⁴⁾,10⁽⁴⁾,15⁽⁴⁾,20⁽⁴⁾-tetra-tert-butyl-5⁽⁶⁾-methyl-5,10,15,20-tetraphenylporphyrin-2H)2O]

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Technology Process of [Fe(5⁽²⁾-N-(4-aza-18-crown-6)methyl-5⁽⁴⁾,10⁽⁴⁾,15⁽⁴⁾,20⁽⁴⁾-tetra-tert-butyl-5⁽⁶⁾-methyl-5,10,15,20-tetraphenylporphyrin-2H)2O]

There total 1 articles about [Fe(5⁽²⁾-N-(4-aza-18-crown-6)methyl-5⁽⁴⁾,10⁽⁴⁾,15⁽⁴⁾,20⁽⁴⁾-tetra-tert-butyl-5⁽⁶⁾-methyl-5,10,15,20-tetraphenylporphyrin-2H)2O] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

[FeCl(5(2)-N-(4-aza-18-crown-6)methyl-5(4),10(4),15(4),20(4)-tetra-tert-butyl-5(6)-methyl-5,10,15,20-tetraphenylporphyrin-2H)] + sodium hydroxide (1310-73-2) → [Fe(5(2)-N-(4-aza-18-crown-6)methyl-5(4),10(4),15(4),20(4)-tetra-tert-butyl-5(6)-methyl-5,10,15,20-tetraphenylporphyrin-2H)2O] (936131-20-3)

Guidance literature:

In dichloromethane; water; a soln. of complex in CH2Cl2 was shaked with a 2 M soln. aq. NaOH; the organic layer was sepd., dried over anhydrous MgSO4, evapd.;

DOI:10.1021/ja064984p

upstream raw materials:

sodium hydroxide

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