1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazido-4',6'-O-benzylidene-5''-carboxyparomomycin

Base Information

• Chemical Name: 1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazido-4',6'-O-benzylidene-5''-carboxyparomomycin
• CAS No.: 931406-42-7
• Molecular Formula: C₃₀H₃₇N₁₅O₁₅
• Molecular Weight: 847.715

Synonyms:1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazido-4',6'-O-benzylidene-5''-carboxyparomomycin

Chemical Property of 1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazido-4',6'-O-benzylidene-5''-carboxyparomomycin

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Technology Process of 1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazido-4',6'-O-benzylidene-5''-carboxyparomomycin

There total 1 articles about 1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazido-4',6'-O-benzylidene-5''-carboxyparomomycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

4',6‘-O-benzylidene-1,2',2''',3,6'''-pentaazidoparomomycin (875125-34-1) → 1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazido-4',6'-O-benzylidene-5''-carboxyparomomycin (931406-42-7)

Guidance literature:

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene; In water; acetonitrile; at 23 ℃; for 48h;

DOI:10.1016/j.carres.2006.09.014

Reference yield: 84.0%

1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazido-4',6'-O-benzylidene-5''-carboxyparomomycin (931406-42-7) → 4',6'-O-benzylidene-5''-carboxyparomomycin

Guidance literature:

With sodium hydroxide; trimethylphosphane; In tetrahydrofuran; water; at 50 ℃;

DOI:10.1016/j.carres.2006.09.014

Reference yield: 76.0%

1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazido-4',6'-O-benzylidene-5''-carboxyparomomycin (931406-42-7) + acetic anhydride (108-24-7) → 6,3',2'',3''',4'''-penta-O-acetyl-1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazido-4',6'-O-benzylidene-5''-carboxyparomomycin

Guidance literature:

With pyridine; at 25 ℃; for 18h;

DOI:10.1016/j.carres.2006.09.014

upstream raw materials:

4',6‘-O-benzylidene-1,2',2''',3,6'''-pentaazidoparomomycin

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