2,5-Methanothiopyrano[3,2-b]pyrrole,octahydro-1-methyl-(9CI)

Base Information

Chemical Name:2,5-Methanothiopyrano[3,2-b]pyrrole,octahydro-1-methyl-(9CI)
CAS No.:788767-51-1
Molecular Formula:C₉H₁₅NS
Molecular Weight:169.291
Hs Code.:
Mol file:788767-51-1.mol

Synonyms:2,5-Methanothiopyrano[3,2-b]pyrrole,octahydro-1-methyl-(9CI)

Suppliers and Price of 2,5-Methanothiopyrano[3,2-b]pyrrole,octahydro-1-methyl-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-Methanothiopyrano[3,2-b]pyrrole,octahydro-1-methyl-(9CI)

Chemical Property:

Purity/Quality:

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Technology Process of 2,5-Methanothiopyrano[3,2-b]pyrrole,octahydro-1-methyl-(9CI)

There total 6 articles about 2,5-Methanothiopyrano[3,2-b]pyrrole,octahydro-1-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 8-chloro-1-methyl-octahydro-2,5-methano-thiopyrano[3,2-b]pyrrole

: 791727-67-8
5-methyl-octahydro-2,6-cyclo-thiopyrano[3,2-b]pyridine

: 788767-51-1
1-methyl-octahydro-2,5-methano-thiopyrano[3,2-b]pyrrole

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; Ambient temperature;
DOI:10.1002/hlca.19760590832

Reference yield:

: 62545-76-0,62562-09-8
5-methyl-octahydro-2,6-cyclo-thiopyrano[3,2-b]pyridin-4-ol

: 788767-51-1
1-methyl-octahydro-2,5-methano-thiopyrano[3,2-b]pyrrole

Guidance literature:: Multi-step reaction with 4 steps

1: Py / 3 h / 70 °C

2: aq. K₂CO₃ / methanol / 1 h / 45 °C

3: SOCl₂ / 0.5 h / Heating

4: LiAlH₄ / diethyl ether / Ambient temperature

With pyridine; lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; In methanol; diethyl ether;
DOI:10.1002/hlca.19760590832

Reference yield:

: 62545-52-2
1-methyl-octahydro-2,5-methano-thiopyrano[3,2-b]pyrrol-8-ol

: 788767-51-1
1-methyl-octahydro-2,5-methano-thiopyrano[3,2-b]pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 0.5 h / Heating

2: LiAlH₄ / diethyl ether / Ambient temperature

With lithium aluminium tetrahydride; thionyl chloride; In diethyl ether;
DOI:10.1002/hlca.19760590832