C₆₄H₆₀N₄Si₄Zn

Base Information

Chemical Name:C₆₄H₆₀N₄Si₄Zn
CAS No.:1361092-36-5
Molecular Formula:C₆₄H₆₀N₄Si₄Zn
Molecular Weight:1062.94
Hs Code.:

C<sub>64</sub>H<sub>60</sub>N<sub>4</sub>Si<sub>4</sub>Zn

Synonyms:C₆₄H₆₀N₄Si₄Zn

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Chemical Property of C₆₄H₆₀N₄Si₄Zn

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Technology Process of C₆₄H₆₀N₄Si₄Zn

There total 4 articles about C₆₄H₆₀N₄Si₄Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₄H₆₂N₄Si₄

: 1361092-36-5
C₆₄H₆₀N₄Si₄Zn

Guidance literature:: With zinc diacetate; In methanol; dichloromethane; at 25 ℃; for 1h;
DOI:10.1002/chem.201101884

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 1361092-36-5
C₆₄H₆₀N₄Si₄Zn

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 16 h / 50 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 12 h / 25 °C

2.2: 4 h

3.1: zinc diacetate / methanol; dichloromethane / 1 h / 25 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; zinc diacetate; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; 1.1: Sonogashira coupling;
DOI:10.1002/chem.201101884

Reference yield:

: 77123-58-1
2-[2-(trimethylsilyl)ethynyl]benzaldehyde

: 1361092-36-5
C₆₄H₆₀N₄Si₄Zn

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 12 h / 25 °C

1.2: 4 h

2.1: zinc diacetate / methanol; dichloromethane / 1 h / 25 °C

With zinc diacetate; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1002/chem.201101884