Technology Process of C25H32N2OS
There total 6 articles about C25H32N2OS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
tetrahydrofuran;
at 40 - 60 ℃;
for 42h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium hydroxide / ethanol / 2 h / Reflux
2.1: pyridine / 2 h / Reflux
3.1: vanadium pentoxide; hydrogen; platinum on carbon / tetrahydrofuran / 25 °C
4.1: acetic acid / 3 h / Reflux
4.2: 22 h / Reflux
5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 40 °C / Inert atmosphere
5.2: 42 h / 40 - 60 °C
With
pyridine; vanadium pentoxide; platinum on carbon; hydrogen; sodium hydride; acetic acid; potassium hydroxide;
In
tetrahydrofuran; ethanol; mineral oil;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / 2 h / Reflux
2.1: vanadium pentoxide; hydrogen; platinum on carbon / tetrahydrofuran / 25 °C
3.1: acetic acid / 3 h / Reflux
3.2: 22 h / Reflux
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 40 °C / Inert atmosphere
4.2: 42 h / 40 - 60 °C
With
pyridine; vanadium pentoxide; platinum on carbon; hydrogen; sodium hydride; acetic acid;
In
tetrahydrofuran; mineral oil;