phenylphosphine borane

Base Information

Chemical Name:phenylphosphine borane
CAS No.:666857-23-4
Molecular Formula:C₆H₈BP
Molecular Weight:121.914
Hs Code.:

Synonyms:phenylphosphine borane

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Chemical Property of phenylphosphine borane

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Technology Process of phenylphosphine borane

There total 5 articles about phenylphosphine borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 666857-16-5
(methyl)2NHBH₂PH(phenyl)BH₃

: 666857-23-4
phenylphosphine borane

Guidance literature:: In neat (no solvent); byproducts: [(CH3)2NBH2]2; N2; heating neat sample of amine-phosphine-borate at 130°C for 2 h; evacuation at 25°C for 24 h;
DOI:10.1021/ic034938f

Reference yield: 75.0%

: diphenylphosphine-borane complex

: 666857-23-4
phenylphosphine borane

Guidance literature:: di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium; In neat (no solvent); (N2); 90°C, 3 h, 130°C, 3 h; dissoln. (Ch2Cl29, filtration, pptn. with hexanes, washing (hexanes), decantation), drying (vac., 50°C, 48 h); high molecular weight polymer (M(w) = 31000);
DOI:10.1002/(SICI)1521-3773(19991115)38:22<3321::AID-ANIE3321>3.0.CO;2-0

Reference yield: 63.0%

: 6996-29-8
phenylphosphine-borane

: 666857-23-4
phenylphosphine borane

Guidance literature:: tris(pentafluorophenyl)borate; In toluene; a soln. of P compd. slowly added to a soln. of catalyst (under neutral gas, in dry solvent), 20°C for 3 d (or 90°C for 3 h);
DOI:10.1039/b206559b