C₄₂H₆₃NO₉SSi₂

Base Information

Chemical Name:C₄₂H₆₃NO₉SSi₂
CAS No.:1622094-29-4
Molecular Formula:C₄₂H₆₃NO₉SSi₂
Molecular Weight:814.201
Hs Code.:

C<sub>42</sub>H<sub>63</sub>NO<sub>9</sub>SSi<sub>2</sub>

Synonyms:C₄₂H₆₃NO₉SSi₂

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Chemical Property of C₄₂H₆₃NO₉SSi₂

Chemical Property:

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Technology Process of C₄₂H₆₃NO₉SSi₂

There total 14 articles about C₄₂H₆₃NO₉SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1622094-37-4
C₄₀H₆₁NO₈SSi₂

: 108-24-7
acetic anhydride

: 1622094-29-4
C₄₂H₆₃NO₉SSi₂

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/chem.201402323

Reference yield:

: 179260-96-9
4-methoxy-3-(triisopropylsilyloxy)-benzaldehyde

: 1622094-29-4
C₄₂H₆₃NO₉SSi₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: silver nitrate; iodine / dichloromethane / 14 h / 20 °C / Inert atmosphere

2.1: copper dichloride; tert.-butylhydroperoxide / acetonitrile; water / 16 h / 20 - 50 °C

3.1: thionyl chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere; Reflux

4.1: water; tetrahydrofuran / 0.08 h

4.2: 2 h / 0 °C

5.1: lithium iodide monohydrate / ethyl acetate / 48 h / 20 °C / Reflux

6.1: [bis(acetoxy)iodo]benzene / dichloromethane / 0.17 h / 20 °C

7.1: potassium hydroxide / water; methanol / 0.25 h / -20 °C

8.1: 2,6-dimethylpyridine / dichloromethane / 3 h / 20 °C / Inert atmosphere

9.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

10.1: triethylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

11.1: lithium borohydride / tetrahydrofuran / 6 h / -78 °C / Inert atmosphere

12.1: triethylamine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; tert.-butylhydroperoxide; dmap; lithium borohydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; lithium iodide monohydrate; [bis(acetoxy)iodo]benzene; iodine; silver nitrate; triethylamine; potassium hydroxide; copper dichloride; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetonitrile; 4.1: |Schotten-Baumann Reaction;
DOI:10.1002/chem.201402323

Reference yield:

: 1622094-28-3
C₄₀H₅₉NO₈SSi₂

: 1622094-29-4
C₄₂H₆₃NO₉SSi₂

Guidance literature:: Multi-step reaction with 2 steps

1: lithium borohydride / tetrahydrofuran / 6 h / -78 °C / Inert atmosphere

2: triethylamine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

With dmap; lithium borohydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201402323