C₅₄H₁₀₃BN₃PSi₄

Base Information

• Chemical Name: C₅₄H₁₀₃BN₃PSi₄
• CAS No.: 906543-39-3
• Molecular Formula: C₅₄H₁₀₃BN₃PSi₄
• Molecular Weight: 948.559
• Mol file: 906543-39-3.mol

Synonyms:C₅₄H₁₀₃BN₃PSi₄

Chemical Property of C₅₄H₁₀₃BN₃PSi₄

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₅₄H₁₀₃BN₃PSi₄

There total 2 articles about C₅₄H₁₀₃BN₃PSi₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-[(3-azido-propyl)-bis-(3-tripropylsilanyl-propyl)-silanyl]-3-tripropylsilanyl-propane (881035-91-2) + propargyl(diphenyl)phosphine borane complex (906543-22-4) → C54H103BN3PSi4 (906543-39-3)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In tetrahydrofuran; water; at 20 ℃; for 12h;

DOI:10.1021/ol061015q

Reference yield:

(diphenyl)phosphine borane complex → C54H103BN3PSi4 (906543-39-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / n-butyllithium / tetrahydrofuran; hexane; toluene / 0.25 h / -72 °C

2: copper(II) sulfate; sodium ascorbate / tetrahydrofuran; H₂O / 12 h / 20 °C

With n-butyllithium; copper(II) sulfate; sodium L-ascorbate; In tetrahydrofuran; hexane; water; toluene;

DOI:10.1021/ol061015q

Reference yield: 95.0%

C54H103BN3PSi4 (906543-39-3) → 4-[(diphenylphosphanyl)-methyl]-1-{3-[tris-(3-tripropylsilanyl-propyl)-silanyl]-propyl}-1H-[1,2,3]triazole

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; at 70 ℃; for 3h;

DOI:10.1021/ol061015q

upstream raw materials:

1-[(3-azido-propyl)-bis-(3-tripropylsilanyl-propyl)-silanyl]-3-tripropylsilanyl-propane

propargyl(diphenyl)phosphine borane complex