2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)ethoxy)ethoxy)ethyl azide

Base Information

Chemical Name:2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)ethoxy)ethoxy)ethyl azide
CAS No.:1061632-48-1
Molecular Formula:C₃₅H₄₆N₆O₉S₂
Molecular Weight:758.917
Hs Code.:

Synonyms:2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)ethoxy)ethoxy)ethyl azide

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Chemical Property of 2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)ethoxy)ethoxy)ethyl azide

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Technology Process of 2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)ethoxy)ethoxy)ethyl azide

There total 1 articles about 2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)ethoxy)ethoxy)ethyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.4%

: 134179-38-7
2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethylamine

: 62796-29-6
rhodamine B sulfonyl chloride

: 1061632-48-1
2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)ethoxy)ethoxy)ethyl azide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 22h; Inert atmosphere;

Reference yield: 98.0%

: 1061632-48-1
2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)ethoxy)ethoxy)ethyl azide

: N-(2-propyn-1-yl) 3-(4-tosyl-4,8-diazacyclononyn-8-ylcarbonyl)propionamide

: 1-(2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)-ethoxy)ethoxy)ethyl)-4-(3-(4-tosyl-4,8-diazacyclononyn-8-ylcarbonyl)propionylaminomethyl)1H-1,2,3-triazole

Guidance literature:: N-(2-propyn-1-yl) 3-(4-tosyl-4,8-diazacyclononyn-8-ylcarbonyl)propionamide; With tetrakis(acetonitrile)copper(I)tetrafluoroborate; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)ethoxy)ethoxy)ethyl azide; With 3-[4-[[bis[[1-(3-hydroxypropyl)triazol-4-yl]methyl]amino]methyl]triazol-1-yl]propan-1-ol; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

With disodium ethylenediamine tetraacetic acid; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/C9CC01113G

Reference yield: 94.0%

: 1061632-48-1
2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)ethoxy)ethoxy)ethyl azide

: 57341-09-0
1-azido-2,6-dichlorobenzene

: 4-(diphenylphosphino)-N-(2-propyn-1-yl)benzamide

: 2,6-dichloro-N-(4-(((1-(2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)ethoxy)ethoxy)ethyl)-1H-1,2,3-triazol-4-yl)methyl)carbamoylphenyl)diphenylphosphoranylidene)aniline

Guidance literature:: 4-(diphenylphosphino)-N-(2-propyn-1-yl)benzamide; With tetrakis(acetonitrile)copper(I)tetrafluoroborate; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

2-(2-(2-(2-(4-(3,6-bis(diethylamino)xanthylium-9-yl)-3-sulfonatobenzenesulfonamido)ethoxy)ethoxy)ethoxy)ethyl azide; With tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

1-azido-2,6-dichlorobenzene; In dichloromethane; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1039/d0cc06551j