N-butyryl-N'-<2-<2-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>ethoxy>ethyl>sarcosinamide

Base Information

Chemical Name:N-butyryl-N'-<2-<2-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>ethoxy>ethyl>sarcosinamide
CAS No.:162687-87-8
Molecular Formula:C₂₈H₃₆N₄O₅S
Molecular Weight:540.684
Hs Code.:

Synonyms:N-butyryl-N'-<2-<2-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>ethoxy>ethyl>sarcosinamide

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Chemical Property of N-butyryl-N'-<2-<2-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>ethoxy>ethyl>sarcosinamide

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Technology Process of N-butyryl-N'-<2-<2-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>ethoxy>ethyl>sarcosinamide

There total 3 articles about N-butyryl-N'-<2-<2-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>ethoxy>ethyl>sarcosinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 39908-69-5
4,5-bis(4-methoxyphenyl)-2-mercapto-1H-imidazole

: 162687-86-7
N'-[2-(2-bromoethoxy)-ethyl]-N-butyryl-sarcosinamide

: 162687-87-8
N-butyryl-N'-<2-<2-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>ethoxy>ethyl>sarcosinamide

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; In tetrahydrofuran; for 2h; Heating;
DOI:10.1021/jm00007a004

Reference yield:

: 162688-31-5
N-butyrylsarcosine

: 162687-87-8
N-butyryl-N'-<2-<2-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>ethoxy>ethyl>sarcosinamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 1-hydroxybenzotriazole hydrate, 2.) dicyclohexylcarbodiimide / 1.) DMF, RT, 20 min, 2.) DMF, RT, 48 h

2: 54 percent / Ph₃P, CBr₄ / CH₂Cl₂ / 3 h / Ambient temperature

3: 74 percent / K₂CO₃, tetra-n-butylammonium iodide / tetrahydrofuran / 2 h / Heating

With carbon tetrabromide; tetra-(n-butyl)ammonium iodide; potassium carbonate; 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00007a004

Reference yield:

: 162687-85-6
N-butyryl-N'-<2-(2-hydroxyethoxy)ethyl>sarcosinamide

: 162687-87-8
N-butyryl-N'-<2-<2-<<4,5-bis(4-methoxyphenyl)-1H-imidazol-2-yl>thio>ethoxy>ethyl>sarcosinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / Ph₃P, CBr₄ / CH₂Cl₂ / 3 h / Ambient temperature

2: 74 percent / K₂CO₃, tetra-n-butylammonium iodide / tetrahydrofuran / 2 h / Heating

With carbon tetrabromide; tetra-(n-butyl)ammonium iodide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00007a004