2,3-Dihydro-N-<4-(1,1-dimethylethyl)phenylmethyl>-N,2,2-trimethyl-7-benzofurancarboxamid

Base Information

Chemical Name:2,3-Dihydro-N-<4-(1,1-dimethylethyl)phenylmethyl>-N,2,2-trimethyl-7-benzofurancarboxamid
CAS No.:149530-60-9
Molecular Formula:C₂₃H₂₉NO₂
Molecular Weight:351.489
Hs Code.:

Synonyms:2,3-Dihydro-N-<4-(1,1-dimethylethyl)phenylmethyl>-N,2,2-trimethyl-7-benzofurancarboxamid

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Chemical Property of 2,3-Dihydro-N-<4-(1,1-dimethylethyl)phenylmethyl>-N,2,2-trimethyl-7-benzofurancarboxamid

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Technology Process of 2,3-Dihydro-N-<4-(1,1-dimethylethyl)phenylmethyl>-N,2,2-trimethyl-7-benzofurancarboxamid

There total 2 articles about 2,3-Dihydro-N-<4-(1,1-dimethylethyl)phenylmethyl>-N,2,2-trimethyl-7-benzofurancarboxamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42327-95-7
2,3-Dihydro-2,2-dimethyl-7-benzofurancarbonsaeure

: 149530-60-9
2,3-Dihydro-N-<4-(1,1-dimethylethyl)phenylmethyl>-N,2,2-trimethyl-7-benzofurancarboxamid

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / toluene / 3 h / Heating

2: triethylamine / toluene / 1 h / Ambient temperature

With thionyl chloride; triethylamine; In toluene;
DOI:10.1002/ardp.19933260608

Reference yield:

: 499785-51-2
2,2-dimethyl-2,3-dihydro-1-benzofuran-7-carbonyl chloride

: 101846-35-9
N-4-(1,1-Dimethylethyl)-N-methyl-benzolmethanamin hydrochlorid

: 149530-60-9
2,3-Dihydro-N-<4-(1,1-dimethylethyl)phenylmethyl>-N,2,2-trimethyl-7-benzofurancarboxamid

Guidance literature:: With triethylamine; In toluene; for 1h; Yield given; Ambient temperature;
DOI:10.1002/ardp.19933260608

Reference yield: 93.0%

: 149530-60-9
2,3-Dihydro-N-<4-(1,1-dimethylethyl)phenylmethyl>-N,2,2-trimethyl-7-benzofurancarboxamid

: 2,3-Dihydro-N-<4-(1,1-dimethylethyl)phenylmethyl>-N,2,2-trimethyl-7-benzofuranmethanamin-Hydrochlorid

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene; for 1h; Ambient temperature;
DOI:10.1002/ardp.19933260608