Benzyl 2,4-di-O-benzyl-2'-O-methyllecanorate

Base Information

• Chemical Name: Benzyl 2,4-di-O-benzyl-2'-O-methyllecanorate
• CAS No.: 171624-62-7
• Molecular Formula: C₃₈H₃₄O₇
• Molecular Weight: 602.684
• Mol file: 171624-62-7.mol

Synonyms:Benzyl 2,4-di-O-benzyl-2'-O-methyllecanorate

Chemical Property of Benzyl 2,4-di-O-benzyl-2'-O-methyllecanorate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of Benzyl 2,4-di-O-benzyl-2'-O-methyllecanorate

There total 1 articles about Benzyl 2,4-di-O-benzyl-2'-O-methyllecanorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

2,4-bis-(benzyloxy)-6-methylbenzoic acid (7141-98-2) + benzyl 4-hydroxy-2-methoxy-6-methylbenzoate (70342-24-4) → Benzyl 2,4-di-O-benzyl-2'-O-methyllecanorate (171624-62-7)

Guidance literature:

With trifluoroacetic anhydride; In toluene; for 24h; Ambient temperature;

DOI:10.1071/CH9951761

Reference yield: 90.0%

Benzyl 2,4-di-O-benzyl-2'-O-methyllecanorate (171624-62-7) → 2'-O-Methyllecanoric acid (171624-63-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 24h;

DOI:10.1071/CH9951761

Reference yield:

Benzyl 2,4-di-O-benzyl-2'-O-methyllecanorate (171624-62-7) → Benzyl 2'-O-methyllecanorate (171624-64-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / H₂ / Pd/C / ethyl acetate / 24 h

2: 86 percent / KHCO₃ / dimethylformamide / 48 h

With hydrogen; potassium hydrogencarbonate; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1071/CH9951761

upstream raw materials:

2,4-bis-(benzyloxy)-6-methylbenzoic acid

benzyl 4-hydroxy-2-methoxy-6-methylbenzoate

Downstream raw materials:

2'-O-Methyllecanoric acid

Benzyl 2'-O-methyllecanorate

Benzyl 2,4-di-O-benzyl-2''-methylgyrophorate