C₅₀H₅₁ClO₆

Base Information

Chemical Name:C₅₀H₅₁ClO₆
CAS No.:1161430-56-3
Molecular Formula:C₅₀H₅₁ClO₆
Molecular Weight:783.404
Hs Code.:

C<sub>50</sub>H<sub>51</sub>ClO<sub>6</sub>

Synonyms:C₅₀H₅₁ClO₆

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Chemical Property of C₅₀H₅₁ClO₆

Chemical Property:

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Technology Process of C₅₀H₅₁ClO₆

There total 11 articles about C₅₀H₅₁ClO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1413373-23-5
C₅₀H₄₉ClO₅

: 1161430-56-3
C₅₀H₅₁ClO₆

Guidance literature:: C₅₀H₄₉ClO₅; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere; Reflux;

With sodium hydroxide; In tetrahydrofuran; water; at 0 ℃;

With dihydrogen peroxide; In tetrahydrofuran; water; at 25 - 30 ℃;

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 1161430-56-3
C₅₀H₅₁ClO₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene; tetrahydrofuran / 3.67 h / 0 - 50 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

2.2: 2.25 h / -78 - 20 °C

3.1: L-proline / dimethyl sulfoxide / 8 h / 50 °C

4.1: pyridine; trichlorophosphate / 0 - 20 °C

5.1: magnesium / ethylene dibromide / tetrahydrofuran / 1 h / Inert atmosphere; Reflux

5.2: 3 h / 25 °C / Inert atmosphere

6.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2.5 h / -20 °C / Inert atmosphere

7.1: dimethylsulfide borane complex / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere; Reflux

7.2: 0 °C

7.3: 25 - 30 °C

With pyridine; triethylsilane; oxalyl dichloride; dimethylsulfide borane complex; boron trifluoride diethyl etherate; magnesium; dimethyl sulfoxide; L-proline; trichlorophosphate; ethylene dibromide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene;

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 1161430-56-3
C₅₀H₅₁ClO₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 0 °C

1.3: cooling with ice

2.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C

3.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C

3.2: -78 - 0 °C

4.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C

5.1: magnesium / ethylene dibromide / tetrahydrofuran / 1 h / Inert atmosphere; Reflux

5.2: 3 h / 25 °C / Inert atmosphere

6.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2.5 h / -20 °C / Inert atmosphere

7.1: dimethylsulfide borane complex / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere; Reflux

7.2: 0 °C

7.3: 25 - 30 °C

With triethylsilane; sodium tetrahydroborate; n-butyllithium; dimethylsulfide borane complex; boron trifluoride diethyl etherate; potassium carbonate; magnesium; dimethyl sulfoxide; trifluoroacetic anhydride; 18-crown-6 ether; ethylene dibromide; In tetrahydrofuran; hexane; dichloromethane; toluene;