carbonic acid allyl ester 6-bromo-2-methyl-5-phenylsulfanyl-cyclohexa-1,5-dienyl ester

Base Information

Chemical Name:carbonic acid allyl ester 6-bromo-2-methyl-5-phenylsulfanyl-cyclohexa-1,5-dienyl ester
CAS No.:900493-57-4
Molecular Formula:C₁₇H₁₇BrO₃S
Molecular Weight:381.29
Hs Code.:

Synonyms:carbonic acid allyl ester 6-bromo-2-methyl-5-phenylsulfanyl-cyclohexa-1,5-dienyl ester

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Chemical Property of carbonic acid allyl ester 6-bromo-2-methyl-5-phenylsulfanyl-cyclohexa-1,5-dienyl ester

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Technology Process of carbonic acid allyl ester 6-bromo-2-methyl-5-phenylsulfanyl-cyclohexa-1,5-dienyl ester

There total 3 articles about carbonic acid allyl ester 6-bromo-2-methyl-5-phenylsulfanyl-cyclohexa-1,5-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-bromo-6-methyl-3-phenylsulfanyl-cyclohex-2-enone

: 2937-50-0
Allyl chloroformate

: 900493-57-4
carbonic acid allyl ester 6-bromo-2-methyl-5-phenylsulfanyl-cyclohexa-1,5-dienyl ester

Guidance literature:: 2-bromo-6-methyl-3-phenylsulfanyl-cyclohex-2-enone; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

Allyl chloroformate; In tetrahydrofuran;
DOI:10.1002/anie.200504421

Reference yield:

: 108-98-5
thiophenol

: 900493-57-4
carbonic acid allyl ester 6-bromo-2-methyl-5-phenylsulfanyl-cyclohexa-1,5-dienyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₃N; methanesulfonyl chloride / acetonitrile

1.2: Et₃N / acetonitrile

2.1: LDA / tetrahydrofuran / -78 °C

2.2: tetrahydrofuran / -20 °C

3.1: LDA / tetrahydrofuran / -78 °C

3.2: tetrahydrofuran

With methanesulfonyl chloride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; acetonitrile;
DOI:10.1002/anie.200504421

Reference yield:

: 470458-71-0
2-bromo-3-(phenylsulfanyl)cyclohex-2-en-1-one

: 900493-57-4
carbonic acid allyl ester 6-bromo-2-methyl-5-phenylsulfanyl-cyclohexa-1,5-dienyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA / tetrahydrofuran / -78 °C

1.2: tetrahydrofuran / -20 °C

2.1: LDA / tetrahydrofuran / -78 °C

2.2: tetrahydrofuran

With lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1002/anie.200504421