Technology Process of methyl 9-mercaptononanoate
There total 1 articles about methyl 9-mercaptononanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dimethylformamide / 0.5 h / Ambient temperature
2: NaH / methanol / 0.17 h / 0 °C
With
sodium hydride;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00121a028
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrazine hydrate / ethanol / 16 h / Reflux
2: acetic acid / methanol / 2 h / 20 °C / Inert atmosphere
With
hydrazine hydrate; acetic acid;
In
methanol; ethanol;
DOI:10.1021/ja106486b
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrazine hydrate / ethanol / 16 h / Reflux
2.1: acetic acid / methanol / 2 h / 20 °C / Inert atmosphere
3.1: sodium methylate / methanol; dichloromethane / 2 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: tetrakis(actonitrile)copper(I) hexafluorophosphate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / tetrahydrofuran; methanol; dichloromethane / 16 h / 20 °C / Inert atmosphere
With
tetrakis(actonitrile)copper(I) hexafluorophosphate; sodium methylate; hydrazine hydrate; acetic acid; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1021/ja106486b
