2-(tert-butyldimethylsilyloxy)-3-(4-methylphenylsulfonylamido)propanal

Base Information

Chemical Name:2-(tert-butyldimethylsilyloxy)-3-(4-methylphenylsulfonylamido)propanal
CAS No.:718633-53-5
Molecular Formula:C₁₆H₂₇NO₄SSi
Molecular Weight:357.546
Hs Code.:

Synonyms:2-(tert-butyldimethylsilyloxy)-3-(4-methylphenylsulfonylamido)propanal

Suppliers and Price of 2-(tert-butyldimethylsilyloxy)-3-(4-methylphenylsulfonylamido)propanal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(tert-butyldimethylsilyloxy)-3-(4-methylphenylsulfonylamido)propanal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(tert-butyldimethylsilyloxy)-3-(4-methylphenylsulfonylamido)propanal

There total 3 articles about 2-(tert-butyldimethylsilyloxy)-3-(4-methylphenylsulfonylamido)propanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: N-[2-(tert-butyl-dimethyl-silanyloxy)-pent-3-enyl]-4-methyl-benzenesulfonamide

: 718633-53-5
2-(tert-butyldimethylsilyloxy)-3-(4-methylphenylsulfonylamido)propanal

Guidance literature:: N-[2-(tert-butyl-dimethyl-silanyloxy)-pent-3-enyl]-4-methyl-benzenesulfonamide; With ozone; In dichloromethane; at -78 ℃;

With dimethylsulfide; In dichloromethane; for 2h;
DOI:10.1021/jo030360f

Reference yield:

: 144422-87-7
(E)-N-(2-hydroxypent-3-en-1-yl)-4-methylbenzenesulfonamide

: 718633-53-5
2-(tert-butyldimethylsilyloxy)-3-(4-methylphenylsulfonylamido)propanal

Guidance literature:: Multi-step reaction with 2 steps

1.1: 76 percent / 2,6-lutidine / CH₂Cl₂ / 1 h

2.1: ozone / CH₂Cl₂ / -78 °C

2.2: 93 percent / Me₂S / CH₂Cl₂ / 2 h

With 2,6-dimethylpyridine; ozone; In dichloromethane;
DOI:10.1021/jo030360f

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 718633-53-5
2-(tert-butyldimethylsilyloxy)-3-(4-methylphenylsulfonylamido)propanal

Guidance literature:: Multi-step reaction with 3 steps

1.1: 61 percent / pyridine / CH₂Cl₂ / 24 h

2.1: 76 percent / 2,6-lutidine / CH₂Cl₂ / 1 h

3.1: ozone / CH₂Cl₂ / -78 °C

3.2: 93 percent / Me₂S / CH₂Cl₂ / 2 h

With pyridine; 2,6-dimethylpyridine; ozone; In dichloromethane;
DOI:10.1021/jo030360f