C₃₄H₄₀O₆

Base Information

Chemical Name:C₃₄H₄₀O₆
CAS No.:954416-27-4
Molecular Formula:C₃₄H₄₀O₆
Molecular Weight:544.688
Hs Code.:

C<sub>34</sub>H<sub>40</sub>O<sub>6</sub>

Synonyms:C₃₄H₄₀O₆

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Chemical Property of C₃₄H₄₀O₆

Chemical Property:

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Technology Process of C₃₄H₄₀O₆

There total 13 articles about C₃₄H₄₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 954416-29-6
C₂₁H₂₄O₄

: 954416-28-5
C₁₃H₁₈O₃

: 954416-27-4
C₃₄H₄₀O₆

Guidance literature:: C₁₃H₁₈O₃; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; at 0 ℃; for 3h;

C₂₁H₂₄O₄; With dmap; In toluene; at 20 ℃; for 1h; Further stages.;
DOI:10.1016/j.tetlet.2007.07.176

Reference yield:

: C₁₂H₂₂O₆

: 954416-27-4
C₃₄H₄₀O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: NaIO₄ / tetrahydrofuran; H₂O / 1 h / 0 °C

1.2: 70 percent / NaBH₄

2.1: TPP; I₂; imidazole / tetrahydrofuran / 1 h / 90 °C

3.1: Zn / ethanol / 1 h / Heating

4.1: 90 percent / NaH; TBAI / tetrahydrofuran / 2 h / 0 °C

5.1: 90 percent / AcOH; water / tetrahydrofuran / 18 h / 20 °C

6.1: TsCl; Et₃N; DMAP / CH₂Cl₂ / 2 h / 0 °C

6.2: 75 percent / K₂CO₃ / methanol / 6 h / 0 °C

7.1: 88 percent / DIBAL-H / CH₂Cl₂ / 2 h / 0 °C

8.1: Et₃N; 2,4,6-trichlorobenzoyl chloride / tetrahydrofuran / 3 h / 0 °C

8.2: 90 percent / DMAP / toluene / 1 h / 20 °C

With 1H-imidazole; dmap; sodium periodate; 2,4,6-trichlorobenzoyl chloride; water; iodine; thiamine diphosphate; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; acetic acid; triethylamine; p-toluenesulfonyl chloride; zinc; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1016/j.tetlet.2007.07.176

Reference yield:

: 18524-19-1
(S)-1-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-prop-2-en-1-ol

: 954416-27-4
C₃₄H₄₀O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: 90 percent / NaH; TBAI / tetrahydrofuran / 2 h / 0 °C

2.1: 90 percent / AcOH; water / tetrahydrofuran / 18 h / 20 °C

3.1: TsCl; Et₃N; DMAP / CH₂Cl₂ / 2 h / 0 °C

3.2: 75 percent / K₂CO₃ / methanol / 6 h / 0 °C

4.1: 88 percent / DIBAL-H / CH₂Cl₂ / 2 h / 0 °C

5.1: Et₃N; 2,4,6-trichlorobenzoyl chloride / tetrahydrofuran / 3 h / 0 °C

5.2: 90 percent / DMAP / toluene / 1 h / 20 °C

With dmap; 2,4,6-trichlorobenzoyl chloride; water; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; acetic acid; triethylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2007.07.176