1,1,3,3-tetracyclohexyl-2-(3,5-dimethyl-1-pyrazolyl)triphosphane

Base Information

• Chemical Name: 1,1,3,3-tetracyclohexyl-2-(3,5-dimethyl-1-pyrazolyl)triphosphane
• CAS No.: 1372611-52-3
• Molecular Formula: C₂₉H₅₁N₂P₃
• Molecular Weight: 520.659
• Mol file: 1372611-52-3.mol

Synonyms:1,1,3,3-tetracyclohexyl-2-(3,5-dimethyl-1-pyrazolyl)triphosphane

Chemical Property of 1,1,3,3-tetracyclohexyl-2-(3,5-dimethyl-1-pyrazolyl)triphosphane

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1,1,3,3-tetracyclohexyl-2-(3,5-dimethyl-1-pyrazolyl)triphosphane

There total 1 articles about 1,1,3,3-tetracyclohexyl-2-(3,5-dimethyl-1-pyrazolyl)triphosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

Phosphorous Acid Tris(3,5-dimethylpyrazolide) (54877-56-4) + dicyclohexylphosphane (829-84-5) → 1,1,3,3-tetracyclohexyl-2-(3,5-dimethyl-1-pyrazolyl)triphosphane (1372611-52-3)

Guidance literature:

In acetonitrile; at 20 ℃; for 15h; Inert atmosphere;

DOI:10.1039/c2cc18030h

Reference yield: 56.0%

diiron nonacarbonyl (15321-51-4) + 1,1,3,3-tetracyclohexyl-2-(3,5-dimethyl-1-pyrazolyl)triphosphane (1372611-52-3) → ((C6H11)2P)((CO)4FeP(C6H11)2)P(N2C3H(CH3)2) (1372611-53-4)

Guidance literature:

In tetrahydrofuran; byproducts: Fe(CO)5; 12 h, room temp.;

DOI:10.1039/c2cc18030h

upstream raw materials:

Phosphorous Acid Tris(3,5-dimethylpyrazolide)

dicyclohexylphosphane

Downstream raw materials:

((C₆H₁₁)2P)((CO)4FeP(C₆H₁₁)2)P(N₂C₃H(CH₃)2)