4-(4-methoxyphenyl)-6-(p-toluidino)-5-(p-tolyl)-2,3-benzo-1,3a,6a-triazapentalene

Base Information

Chemical Name:4-(4-methoxyphenyl)-6-(p-toluidino)-5-(p-tolyl)-2,3-benzo-1,3a,6a-triazapentalene
CAS No.:627088-42-0
Molecular Formula:C₃₀H₂₆N₄O
Molecular Weight:458.563
Hs Code.:

Synonyms:4-(4-methoxyphenyl)-6-(p-toluidino)-5-(p-tolyl)-2,3-benzo-1,3a,6a-triazapentalene

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Chemical Property of 4-(4-methoxyphenyl)-6-(p-toluidino)-5-(p-tolyl)-2,3-benzo-1,3a,6a-triazapentalene

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Technology Process of 4-(4-methoxyphenyl)-6-(p-toluidino)-5-(p-tolyl)-2,3-benzo-1,3a,6a-triazapentalene

There total 7 articles about 4-(4-methoxyphenyl)-6-(p-toluidino)-5-(p-tolyl)-2,3-benzo-1,3a,6a-triazapentalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 627088-27-1
4-(4-methoxyphenyl)-5-(p-tolyl)-6-[N-(p-tolyl)-N-trifluoroacetyl]amino-2,3-benzo-1,3a,6a-triazapentalene

: 627088-42-0
4-(4-methoxyphenyl)-6-(p-toluidino)-5-(p-tolyl)-2,3-benzo-1,3a,6a-triazapentalene

Guidance literature:: In methanol; for 1h; Heating;
DOI:10.1016/j.tetlet.2003.08.012

Reference yield:

: 133349-85-6
1-(4''-methoxybenzyl)-1H-benzo[d][1.2.3]triazole

: 627088-42-0
4-(4-methoxyphenyl)-6-(p-toluidino)-5-(p-tolyl)-2,3-benzo-1,3a,6a-triazapentalene

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-BuLi / tetrahydrofuran / -78 °C

1.2: tetrahydrofuran

2.1: n-BuLi / tetrahydrofuran / -78 °C

2.2: H₃O⁽¹⁺⁾

3.1: DMSO; oxalyl chloride / CH₂Cl₂ / 2 h / -78 °C

3.2: 69 percent / triethylamine / CH₂Cl₂ / 2 h / -78 °C

4.1: 83 percent / ethanol / 12 h / 20 °C

5.1: 89 percent / tetrahydrofuran / 1 h / 20 °C

6.1: 78 percent / methanol / 1 h / Heating

With n-butyllithium; oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2003.08.012

Reference yield:

: 627087-99-4
3-(benzotriazol-1-yl)-3-(4-methoxyphenyl)-2-(4-tolyl)-2-propenol

: 627088-42-0
4-(4-methoxyphenyl)-6-(p-toluidino)-5-(p-tolyl)-2,3-benzo-1,3a,6a-triazapentalene

Guidance literature:: Multi-step reaction with 4 steps

1.1: DMSO; oxalyl chloride / CH₂Cl₂ / 2 h / -78 °C

1.2: 69 percent / triethylamine / CH₂Cl₂ / 2 h / -78 °C

2.1: 83 percent / ethanol / 12 h / 20 °C

3.1: 89 percent / tetrahydrofuran / 1 h / 20 °C

4.1: 78 percent / methanol / 1 h / Heating

With oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2003.08.012