3,4,6-tri-O-benzyl-1,5-N-[carboxymethylimino]-2-(tetradecanoyl)amino-1,2,5-trideoxy-D-glucitol

Base Information

Chemical Name:3,4,6-tri-O-benzyl-1,5-N-[carboxymethylimino]-2-(tetradecanoyl)amino-1,2,5-trideoxy-D-glucitol
CAS No.:470665-46-4
Molecular Formula:C₄₃H₆₀N₂O₆
Molecular Weight:700.959
Hs Code.:

Synonyms:3,4,6-tri-O-benzyl-1,5-N-[carboxymethylimino]-2-(tetradecanoyl)amino-1,2,5-trideoxy-D-glucitol

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Chemical Property of 3,4,6-tri-O-benzyl-1,5-N-[carboxymethylimino]-2-(tetradecanoyl)amino-1,2,5-trideoxy-D-glucitol

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Technology Process of 3,4,6-tri-O-benzyl-1,5-N-[carboxymethylimino]-2-(tetradecanoyl)amino-1,2,5-trideoxy-D-glucitol

There total 4 articles about 3,4,6-tri-O-benzyl-1,5-N-[carboxymethylimino]-2-(tetradecanoyl)amino-1,2,5-trideoxy-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 470665-44-2
3,4,6-tri-O-benzyl-1,5-N-[(O-tert-butyl-carboxymethyl)imino]-2-(tetradecanoyl)amino-1,2,5-trideoxy-D-glucitol

: 470665-46-4
3,4,6-tri-O-benzyl-1,5-N-[carboxymethylimino]-2-(tetradecanoyl)amino-1,2,5-trideoxy-D-glucitol

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 2h;
DOI:10.1081/CAR-120004331

Reference yield:

: 250737-19-0
3,4,6-tri-O-benzyl-2-[(benzyloxycarbonyl)amino]-1,2,5-trideoxy-1,5-imino-D-glucitol

: 470665-46-4
3,4,6-tri-O-benzyl-1,5-N-[carboxymethylimino]-2-(tetradecanoyl)amino-1,2,5-trideoxy-D-glucitol

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / Cs₂CO₃ / dimethylformamide / 16 h / 20 °C

2: 100 percent / H₂ / Pd/C / ethyl acetate / 1 h / 760 Torr

3: 89 percent / N,N-diisopropylethylamine; PyBOP / CH₂Cl₂ / 0.5 h

4: 100 percent / TFA / 2 h / 20 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; caesium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1081/CAR-120004331

Reference yield:

: 470665-42-0
3,4,6-tri-O-benzyl-2-[(benzyloxycarbonyl)amino]-1,5-N-(O-tert-butyl-carboxymethyl)imino-1,2,5-trideoxy-D-glucitol

: 470665-46-4
3,4,6-tri-O-benzyl-1,5-N-[carboxymethylimino]-2-(tetradecanoyl)amino-1,2,5-trideoxy-D-glucitol

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / Pd/C / ethyl acetate / 1 h / 760 Torr

2: 89 percent / N,N-diisopropylethylamine; PyBOP / CH₂Cl₂ / 0.5 h

3: 100 percent / TFA / 2 h / 20 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1081/CAR-120004331