(3R,17R)-3,17-diphenyl-1,10-bis(p-tolylsulfonyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane

Base Information

Chemical Name:(3R,17R)-3,17-diphenyl-1,10-bis(p-tolylsulfonyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane
CAS No.:150125-94-3
Molecular Formula:C₃₈H₄₆N₂O₈S₂
Molecular Weight:722.924
Hs Code.:

Synonyms:(3R,17R)-3,17-diphenyl-1,10-bis(p-tolylsulfonyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane

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Chemical Property of (3R,17R)-3,17-diphenyl-1,10-bis(p-tolylsulfonyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane

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Technology Process of (3R,17R)-3,17-diphenyl-1,10-bis(p-tolylsulfonyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane

There total 6 articles about (3R,17R)-3,17-diphenyl-1,10-bis(p-tolylsulfonyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120390-75-2
(R)-(+)-α-<(tert-butyldimethylsilyl)oxy>-benzeneacetonitrile

: 150125-94-3
(3R,17R)-3,17-diphenyl-1,10-bis(p-tolylsulfonyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane

Guidance literature:: Multi-step reaction with 4 steps

2: 98 percent / pyridine / 18 h / 5 °C

3: 95 percent / TBAF*3H₂O / tetrahydrofuran / Ambient temperature

4: 1.) NaH / 1.) THF, mineral oil, reflux, 2.) THF, reflux

With pyridine; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo00068a029

Reference yield:

: 72358-83-9,63413-83-2
N,N-bis<2-(2-hydroxyethoxy)ethyl>-4-methylbenzenesulfonamide

: 150125-94-3
(3R,17R)-3,17-diphenyl-1,10-bis(p-tolylsulfonyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / triethylamine / CH₂Cl₂ / 48 h / 5 °C

2: 1.) NaH / 1.) THF, mineral oil, reflux, 2.) THF, reflux

With sodium hydride; triethylamine; In dichloromethane;
DOI:10.1021/jo00068a029

Reference yield:

: 150125-74-9
(R)-1-<<(tert-butyldimethylsilyl)oxy>-1-phenylethan-2-yl>-amine

: 150125-94-3
(3R,17R)-3,17-diphenyl-1,10-bis(p-tolylsulfonyl)-1,10-diaza-4,7,13,16-tetraoxacyclooctadecane

Guidance literature:: Multi-step reaction with 4 steps

2: 98 percent / pyridine / 18 h / 5 °C

3: 95 percent / TBAF*3H₂O / tetrahydrofuran / Ambient temperature

4: 1.) NaH / 1.) THF, mineral oil, reflux, 2.) THF, reflux

With pyridine; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo00068a029