C₆₈H₈₄INO₈

Base Information

Chemical Name:C₆₈H₈₄INO₈
CAS No.:1558035-09-8
Molecular Formula:C₆₈H₈₄INO₈
Molecular Weight:1170.32
Hs Code.:

C<sub>68</sub>H<sub>84</sub>INO<sub>8</sub>

Synonyms:C₆₈H₈₄INO₈

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Chemical Property of C₆₈H₈₄INO₈

Chemical Property:

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Technology Process of C₆₈H₈₄INO₈

There total 11 articles about C₆₈H₈₄INO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1558035-08-7
C₆₉H₈₇NO₇S

: 1558035-09-8
C₆₈H₈₄INO₈

Guidance literature:: With iodonium dicollidine perchlorate; In dichloromethane; at 20 ℃; for 16h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol5002686

Reference yield:

: 1558035-05-4
C₆₀H₇₈O₇

: 1558035-09-8
C₆₈H₈₄INO₈

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

1.3: 1 h / 20 °C / Inert atmosphere

2.1: iodonium dicollidine perchlorate / dichloromethane / 16 h / 20 °C / Inert atmosphere

With sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/ol5002686

Reference yield:

: C₂₀H₃₈O₃

: 1558035-09-8
C₆₈H₈₄INO₈

Guidance literature:: Multi-step reaction with 11 steps

1.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 12 h / 20 °C

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate; N-chloro-succinimide / dichloromethane; water / 12 h / 20 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 2 h / 0 - 20 °C / Inert atmosphere

4.1: acetyl chloride / methanol / 0.5 h / Inert atmosphere

5.1: toluene-4-sulfonic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / dichloromethane; hexane / 3.5 h / -78 - 20 °C / Inert atmosphere

7.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C / Inert atmosphere

7.2: 3 h / 0 - 20 °C / Inert atmosphere

8.1: sodium hydrogencarbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 0.42 h / 20 °C / Inert atmosphere

9.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 16 h / 40 °C / Inert atmosphere

10.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

10.2: 3 h / 20 °C / Inert atmosphere

10.3: 1 h / 20 °C / Inert atmosphere

11.1: iodonium dicollidine perchlorate / dichloromethane / 16 h / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium 10% on activated carbon; potassium tert-butylate; tetrabutyl-ammonium chloride; hydrogen; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; acetyl chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol5002686