2-hydroxyl-3,9-diethoxy-10-methoxy-13-n-octylprotoberberine chloride

Base Information

• Chemical Name: 2-hydroxyl-3,9-diethoxy-10-methoxy-13-n-octylprotoberberine chloride
• CAS No.: 1375475-66-3
• Molecular Formula: C₃₀H₄₀NO₄*Cl
• Molecular Weight: 514.105
• Mol file: 1375475-66-3.mol

Synonyms:2-hydroxyl-3,9-diethoxy-10-methoxy-13-n-octylprotoberberine chloride

Chemical Property of 2-hydroxyl-3,9-diethoxy-10-methoxy-13-n-octylprotoberberine chloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-hydroxyl-3,9-diethoxy-10-methoxy-13-n-octylprotoberberine chloride

There total 1 articles about 2-hydroxyl-3,9-diethoxy-10-methoxy-13-n-octylprotoberberine chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7,8-dihydroberberine (483-15-8) → 2-hydroxyl-3,9-diethoxy-10-methoxy-13-n-octylprotoberberine chloride (1375475-66-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: acetic acid / ethanol / 5 h / 85 - 95 °C

1.2: 0.5 h / 20 °C

2.1: aluminum (III) chloride / dichloromethane / 72 h / 20 °C

3.1: potassium hydroxide / N,N-dimethyl-formamide / 70 °C

With aluminum (III) chloride; acetic acid; potassium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2012.03.012

upstream raw materials:

7,8-dihydroberberine