Pt(2-diphenylphosphinopyridine)2Br₂

Base Information

Chemical Name:Pt(2-diphenylphosphinopyridine)2Br₂
CAS No.:84074-40-8
Molecular Formula:C₃₄H₂₈Br₂N₂P₂Pt
Molecular Weight:881.445
Hs Code.:

Pt(2-diphenylphosphinopyridine)2Br<sub>2</sub>

Synonyms:Pt(2-diphenylphosphinopyridine)2Br₂

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Chemical Property of Pt(2-diphenylphosphinopyridine)2Br₂

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Technology Process of Pt(2-diphenylphosphinopyridine)2Br₂

There total 2 articles about Pt(2-diphenylphosphinopyridine)2Br₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 161816-46-2,38255-47-9
{bis(diphenylphosphino)-2-pyridyl}platinum(II) chloride

: 7558-02-3,7758-02-3
potassium bromide

: 84074-40-8
Pt(2-diphenylphosphinopyridine)2Br₂

Guidance literature:: In ethanol; water; 4h, stirring; filtered, vol. reduced in vac. (rotary evaporator), addn. of water, filtration, washing with hot water, hot ethanol, and ether, vac. drying, elem. anal.;
DOI:10.1021/ja00342a024

Reference yield:

: 37943-90-1
2-(diphenylphosphino)pyridine

: 84074-40-8
Pt(2-diphenylphosphinopyridine)2Br₂

Guidance literature:: Multi-step reaction with 2 steps

1: water; ethanol

2: water; ethanol

In ethanol; water;
DOI:10.1021/ja00342a024

Reference yield: 62.0%

: 73190-78-0
(tetrabutylammonium)[IrBr₂(CO)2]

: 84074-40-8
Pt₂Br₂((C₆H₅)2P(C₅H₄N))2

: 100815-10-9
IrPtBr₃(CO)((C₆H₅)2P(C₅H₄N))2

Guidance literature:: In dichloromethane; soln. of Ir complex was added to soln. of Pt complex under N2; gas evolution occured, soln. became bright yellow; refluxing for 5 h; cooling, dild. with Et2O, standing at room temp., refluxing of ppt. in THF for 4 h, sepn. of solid, recrystallization from CH2Cl2-Et2O; elem. anal.;
DOI:10.1021/om00136a014