(E)-3-octenoic acid benzylamide

Base Information

• Chemical Name: (E)-3-octenoic acid benzylamide
• CAS No.: 133910-57-3
• Molecular Formula: C₁₅H₂₁NO
• Molecular Weight: 231.338
• Mol file: 133910-57-3.mol

Synonyms:(E)-3-octenoic acid benzylamide

Chemical Property of (E)-3-octenoic acid benzylamide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (E)-3-octenoic acid benzylamide

There total 1 articles about (E)-3-octenoic acid benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(E)-oct-3-enoic acid (5163-67-7) + benzylamine (100-46-9) → (E)-3-octenoic acid benzylamide (133910-57-3)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃;

DOI:10.1021/ja710492q

Reference yield:

(E)-3-octenoic acid benzylamide (133910-57-3) → N-benzyl-3-hydroxyoctanamide + N-benzyl-3-hydroxyoctanamide (1016225-20-9) + 4-hydroxy-octanoic acid benzylamide (127839-84-3)

Guidance literature:

(E)-3-octenoic acid benzylamide; With Pinacolborane; di(norbornadiene)rhodium(I) tetrafluoroborate; In tetrahydrofuran; at 40 ℃; for 2h;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 2h; Further stages. Title compound not separated from byproducts.;

DOI:10.1021/ja710492q

upstream raw materials:

(E)-oct-3-enoic acid

benzylamine

Downstream raw materials:

N-benzyl-3-hydroxyoctanamide

4-hydroxy-octanoic acid benzylamide