N-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trimethylbenzenesulfonamide

Base Information

Chemical Name:N-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trimethylbenzenesulfonamide
CAS No.:160422-44-6
Molecular Formula:C₁₉H₂₅NO₄S
Molecular Weight:363.478
Hs Code.:
Mol file:160422-44-6.mol

Synonyms:N-<2-(3,4-dimethoxyphenyl)ethyl>mesitylenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trimethylbenzenesulfonamide

Chemical Property:

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Technology Process of N-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trimethylbenzenesulfonamide

There total 1 articles about N-[2-(3,4-dimethoxyphenyl)ethyl]-2,4,6-trimethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 773-64-8
2-mesitylenesulphonyl chloride

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 160422-44-6
N-<2-(3,4-dimethoxyphenyl)ethyl>mesitylenesulfonamide

Guidance literature:: With dmap; triethylamine; In dichloromethane; Ambient temperature;

Reference yield: 92.0%

: 160422-44-6
N-<2-(3,4-dimethoxyphenyl)ethyl>mesitylenesulfonamide

: 160422-45-7
N-<2-(2-iodo-4,5-dimethoxyphenyl)ethyl>mesitylenesulfonamide

Guidance literature:: With iodine; iodic acid; In methanol; water; for 48h; Heating;

Reference yield:

: 160422-44-6
N-<2-(3,4-dimethoxyphenyl)ethyl>mesitylenesulfonamide

: 2,3,4,5-tetrahydro-3-(mesitylsulfonyl)-7,8-dimethoxy-1-<(Z)-2-(trimethylsilyl)ethylidene>-1H-3-benzazepine

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / I₂, HIO₃ / methanol; H₂O / 48 h / Heating

2: 1.) NaH / 1.) DMF, 0 deg C, 2.) DMF, 50 deg C

3: 90 percent / PPh₃, NaO₂CH / Pd(OAc)2, Pr₄NBr / dimethylformamide / 3 h / 75 - 85 °C

With iodine; sodium formate; iodic acid; sodium hydride; triphenylphosphine; palladium diacetate; tetra-n-propylammonium bromide; In methanol; water; N,N-dimethyl-formamide;