2-chloro-4.6-dinitrophenyl hydrazine

Base Information

Chemical Name:2-chloro-4.6-dinitrophenyl hydrazine
CAS No.:89581-78-2
Molecular Formula:C₆H₅ClN₄O₄
Molecular Weight:232.583
Hs Code.:

Synonyms:2-chloro-4.6-dinitrophenyl hydrazine

Suppliers and Price of 2-chloro-4.6-dinitrophenyl hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-chloro-4.6-dinitrophenyl hydrazine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-chloro-4.6-dinitrophenyl hydrazine

There total 5 articles about 2-chloro-4.6-dinitrophenyl hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.4%

: 100191-51-3
1-chloro-2-iodo-3,5-dinitrobenzene

: 89581-78-2
2-chloro-4.6-dinitrophenyl hydrazine

Guidance literature:: With hydrazine hydrate; In methanol; at 20 ℃; for 28h;
DOI:10.1016/j.tet.2005.03.037

Reference yield:

: 3531-19-9
2-chloro-4,6-dinitroaniline

: 89581-78-2
2-chloro-4.6-dinitrophenyl hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; acetic acid; sulfuric acid / 70 °C

1.2: potassium iodide / H₂O / 0.25 h / 50 °C

2.1: 58.4 percent / hydrazine hydrate / methanol / 28 h / 20 °C

With sulfuric acid; hydrazine hydrate; acetic acid; sodium nitrite; In methanol;
DOI:10.1016/j.tet.2005.03.037