1-(m-nitrophenyl)-4-ethoxycarbonyl-5-[(triphenylphosphoranylidene)amino]-1,2,3-triazole

Base Information

Chemical Name:1-(m-nitrophenyl)-4-ethoxycarbonyl-5-[(triphenylphosphoranylidene)amino]-1,2,3-triazole
CAS No.:272123-43-0
Molecular Formula:C₂₉H₂₄N₅O₄P
Molecular Weight:537.514
Hs Code.:

Synonyms:1-(m-nitrophenyl)-4-ethoxycarbonyl-5-[(triphenylphosphoranylidene)amino]-1,2,3-triazole

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Chemical Property of 1-(m-nitrophenyl)-4-ethoxycarbonyl-5-[(triphenylphosphoranylidene)amino]-1,2,3-triazole

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Technology Process of 1-(m-nitrophenyl)-4-ethoxycarbonyl-5-[(triphenylphosphoranylidene)amino]-1,2,3-triazole

There total 1 articles about 1-(m-nitrophenyl)-4-ethoxycarbonyl-5-[(triphenylphosphoranylidene)amino]-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 603-35-0
triphenylphosphine

: 5-amino-1-(3-nitro-phenyl)-1H-[1,2,3]triazole-4-carboxylic acid ethyl ester

: 272123-43-0
1-(m-nitrophenyl)-4-ethoxycarbonyl-5-[(triphenylphosphoranylidene)amino]-1,2,3-triazole

Guidance literature:: With hexachloroethane; triethylamine; In acetonitrile; for 0.05h; microwave irradiation;
DOI:10.1080/00397910008087150

Reference yield:

: 272123-43-0
1-(m-nitrophenyl)-4-ethoxycarbonyl-5-[(triphenylphosphoranylidene)amino]-1,2,3-triazole

: N-[4-(ethoxycarbonyl)-1-(3'-nitro)phenyl-1,2,3-triazol-5-yl]-O-methyl-N'-phenylisourea

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 4 h / Heating

2: 1 h / Heating

In acetonitrile;
DOI:10.1515/HC.2003.9.4.395

Reference yield:

: 272123-43-0
1-(m-nitrophenyl)-4-ethoxycarbonyl-5-[(triphenylphosphoranylidene)amino]-1,2,3-triazole

: N-[4-(ethoxycarbonyl)-1-(3'-nitro)phenyl-1,2,3,-triazol-5-yl]-O-isopropyl-N'-phenylisourea

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 4 h / Heating

2: 1 h / Heating

In acetonitrile;
DOI:10.1515/HC.2003.9.4.395