C₃₄H₄₄N₂O₈

Base Information

Chemical Name:C₃₄H₄₄N₂O₈
CAS No.:1438408-30-0
Molecular Formula:C₃₄H₄₄N₂O₈
Molecular Weight:608.732
Hs Code.:

C<sub>34</sub>H<sub>44</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₃₄H₄₄N₂O₈

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Chemical Property of C₃₄H₄₄N₂O₈

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Technology Process of C₃₄H₄₄N₂O₈

There total 8 articles about C₃₄H₄₄N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1438408-27-5
C₃₆H₄₆N₂O₉

: 1438408-30-0
C₃₄H₄₄N₂O₈

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-16-2
C₁₄H₂₅NO₄

: 1438408-30-0
C₃₄H₄₄N₂O₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / Cooling with ice; Inert atmosphere

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere

2.2: 8 h / 20 °C / Inert atmosphere

2.3: 3.33 h / 20 °C / Inert atmosphere

3.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

5.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; mercuric triflate / dichloromethane / 10.5 h / -20 °C / Inert atmosphere; Cooling with ice

6.2: 0.5 h / -78 °C / Inert atmosphere

7.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

With 1H-imidazole; C₁₅H₂₆Cl₂CuN₂O₂; iodine; mercuric triflate; diisobutylaluminium hydride; sodium hydrogencarbonate; caesium carbonate; Dess-Martin periodane; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 4.1: |Dess-Martin Oxidation / 5.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-19-5
C₂₅H₃₈N₂O₇

: 1438408-30-0
C₃₄H₄₄N₂O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

3.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; mercuric triflate / dichloromethane / 10.5 h / -20 °C / Inert atmosphere; Cooling with ice

4.2: 0.5 h / -78 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

With C₁₅H₂₆Cl₂CuN₂O₂; mercuric triflate; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; dichloromethane; toluene; 2.1: |Dess-Martin Oxidation / 3.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d