methyl 3-<4-(benzenesulfonylamino)butyl>-6-(1-hydroxyethyl-1-methyl)azulene-1-carboxylate

Base Information

• Chemical Name: methyl 3-<4-(benzenesulfonylamino)butyl>-6-(1-hydroxyethyl-1-methyl)azulene-1-carboxylate
• CAS No.: 150094-22-7
• Molecular Formula: C₂₅H₂₉NO₅S
• Molecular Weight: 455.575

Synonyms:methyl 3-<4-(benzenesulfonylamino)butyl>-6-(1-hydroxyethyl-1-methyl)azulene-1-carboxylate

Chemical Property of methyl 3-<4-(benzenesulfonylamino)butyl>-6-(1-hydroxyethyl-1-methyl)azulene-1-carboxylate

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Technology Process of methyl 3-<4-(benzenesulfonylamino)butyl>-6-(1-hydroxyethyl-1-methyl)azulene-1-carboxylate

There total 2 articles about methyl 3-<4-(benzenesulfonylamino)butyl>-6-(1-hydroxyethyl-1-methyl)azulene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

methyl 3-<4-<(phenylsulfonyl)amino>butyl>-6-isopropylazulene-1-carboxylate (129648-81-3) → methyl 3-<4-(benzenesulfonylamino)butyl>-6-(1-hydroxyethyl-1-methyl)azulene-1-carboxylate (150094-22-7)

Guidance literature:

With oxygen; potassium acetate; In N,N-dimethyl-formamide; at 120 ℃; for 12h; Product distribution; Mechanism; further alkali acetates; other base (tetrabutylammonium hydroxide); further solvents; variation of conditions (temperature, time, and relative amount of base); effect of triphenylphosphine; further 6-alkylazulene derivatives;

DOI:10.1055/s-1994-25706

Reference yield: 24.0%

methyl 3-<4-<(phenylsulfonyl)amino>butyl>-6-isopropylazulene-1-carboxylate (129648-81-3) → methyl 3-<4-(benzenesulfonylamino)butyl>-6-(1-hydroxyethyl-1-methyl)azulene-1-carboxylate (150094-22-7) + methyl 3-<4-(benzenesulfonylamino)butyl>-6-(1-hydroperoxyethyl-1-methyl)azulene-1-carboxylate

Guidance literature:

With tetra(n-butyl)ammonium hydroxide; oxygen; In tetrahydrofuran; methanol; for 72h; Ambient temperature;

DOI:10.1055/s-1994-25706

Reference yield: 87.0%

methyl 3-<4-(benzenesulfonylamino)butyl>-6-(1-hydroxyethyl-1-methyl)azulene-1-carboxylate (150094-22-7) → methyl 3-<4-(benzenesulfonylamino)butyl>-6-isopropenylazulene-1-carboxylate (150094-23-8)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 0.333333h; Heating;

DOI:10.1055/s-1994-25706

upstream raw materials:

methyl 3-<4-<(phenylsulfonyl)amino>butyl>-6-isopropylazulene-1-carboxylate

Downstream raw materials:

methyl 3-<4-(benzenesulfonylamino)butyl>-6-isopropenylazulene-1-carboxylate

methyl 3-<4-(benzenesulfonylamino)butyl>-6-(2-hydroxyethyl-1-methyl)azulene-1-carboxylate

N-{4-[6-(2-Hydroxy-1-methyl-ethyl)-azulen-1-yl]-butyl}-benzenesulfonamide

N-(4-{6-[2-(tert-Butyl-dimethyl-silanyloxy)-1-methyl-ethyl]-azulen-1-yl}-butyl)-benzenesulfonamide

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