Boc-Leu-Glu(OBu^t)-Gly-Pro-Pro-Gln-Lys-N2H3

Base Information

Chemical Name:Boc-Leu-Glu(OBu^t)-Gly-Pro-Pro-Gln-Lys-N2H3
CAS No.:73995-35-4
Molecular Formula:C₅₁H₈₀ClN₁₁O₁₄
Molecular Weight:1106.71
Hs Code.:

Boc-Leu-Glu(OBu<sup>t</sup>)-Gly-Pro-Pro-Gln-Lys<Z(2-Cl)>-N2H3

Synonyms:Boc-Leu-Glu(OBu^t)-Gly-Pro-Pro-Gln-Lys-N2H3

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Boc-Leu-Glu(OBu^t)-Gly-Pro-Pro-Gln-Lys-N2H3

Chemical Property:

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Technology Process of Boc-Leu-Glu(OBu^t)-Gly-Pro-Pro-Gln-Lys-N2H3

There total 16 articles about Boc-Leu-Glu(OBu^t)-Gly-Pro-Pro-Gln-Lys-N2H3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 73995-34-3
Boc-Leu-Glu(OBu^t)-Gly-Pro-Pro-Gln-Lys-OMe

: 73995-35-4
Boc-Leu-Glu(OBu^t)-Gly-Pro-Pro-Gln-Lys-N2H3

Guidance literature:: With hydrazine hydrate; In methanol; for 72h; Ambient temperature;
DOI:10.1246/bcsj.53.192

Reference yield:

: 4666-16-4
5-tert-butyl 1-(2,5-dioxopyrrolidin-1-yl) (S)-2-{[(phenylmethoxy)carbonyl]amino}glutarate

: 73995-35-4
Boc-Leu-Glu(OBu^t)-Gly-Pro-Pro-Gln-Lys-N2H3

Guidance literature:: Multi-step reaction with 5 steps

1: 82.2 percent / 1.) TEA / tetrahydrofuran / 96 h / Ambient temperature

2: H₂ / 5percent palladium-charcoal / methanol / 2.5 h / 35 °C

3: 1.) TEA / CHCl₃ / 72 h / Ambient temperature

4: 1.) N-methylmorpholine, DCC, 2.) 1-hydroxybenzotriazole (HOBt), DCC / tetrahydrofuran / 96 h / 0 - 20 °C

5: 67 percent / NH₂NH₂*H₂O / methanol / 72 h / Ambient temperature

With 4-methyl-morpholine; TEA; hydrogen; benzotriazol-1-ol; hydrazine hydrate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; chloroform;
DOI:10.1246/bcsj.53.192

Reference yield:

: 3392-09-4
Boc-Leu-ONSu

: 73995-35-4
Boc-Leu-Glu(OBu^t)-Gly-Pro-Pro-Gln-Lys-N2H3

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylformamide; CH₂Cl₂ / 1 h / Ambient temperature

2: 1 M NaOH / dioxane / 2 h / Ambient temperature

3: 1.) N-methylmorpholine, DCC, 2.) 1-hydroxybenzotriazole (HOBt), DCC / tetrahydrofuran / 96 h / 0 - 20 °C

4: 67 percent / NH₂NH₂*H₂O / methanol / 72 h / Ambient temperature

With 4-methyl-morpholine; sodium hydroxide; benzotriazol-1-ol; hydrazine hydrate; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.53.192