((C₆H₅CH₂)2S)2B₁₂H₁₀

Base Information

• Chemical Name: ((C₆H₅CH₂)2S)2B₁₂H₁₀
• CAS No.: 320725-95-9
• Molecular Formula: C₂₈H₃₈B₁₂S₂
• Molecular Weight: 568.474
• Mol file: 320725-95-9.mol

Synonyms:((C₆H₅CH₂)2S)2B₁₂H₁₀

Chemical Property of ((C₆H₅CH₂)2S)2B₁₂H₁₀

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ((C₆H₅CH₂)2S)2B₁₂H₁₀

There total 1 articles about ((C₆H₅CH₂)2S)2B₁₂H₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1,12-(SMe2)2B12H10 (158963-31-6) + benzyl chloride (100-44-7) → ((C6H5CH2)2S)2B12H10 (320725-95-9)

Guidance literature:

With sodium iodide; Li; In methylamine; B-complex was placed in flask, Li was added, evacuated, MeNH2 was condensed with liq. N2, warmed to -15°C, soln. was frozen with liq. N2,stirred for 1 h at -15°C, solvent was removed, residue was disso lved in EtOH under N2; filtered off, solvent was removed, MeCN was added, benzyl chloride and NaI was added, refluxed for 2-3.5 h under N2, volatiles were removed, residue was partitioned between CH2Cl2 and water, sepd., dried with MgSO4, recrystd. from MeCN-MeOH;

DOI:10.1021/ic0011011

upstream raw materials:

1,12-(SMe₂)2B₁₂H₁₀

benzyl chloride