(E)-N'-({6-[(diphenylphosphoryl)methyl]pyridin-2-yl}methyl)-N,N-dimethylacetimidamide

Base Information

Chemical Name:(E)-N'-({6-[(diphenylphosphoryl)methyl]pyridin-2-yl}methyl)-N,N-dimethylacetimidamide
CAS No.:1620658-08-3
Molecular Formula:C₂₃H₂₆N₃OP
Molecular Weight:391.453
Hs Code.:

Synonyms:(E)-N'-({6-[(diphenylphosphoryl)methyl]pyridin-2-yl}methyl)-N,N-dimethylacetimidamide

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Chemical Property of (E)-N'-({6-[(diphenylphosphoryl)methyl]pyridin-2-yl}methyl)-N,N-dimethylacetimidamide

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Technology Process of (E)-N'-({6-[(diphenylphosphoryl)methyl]pyridin-2-yl}methyl)-N,N-dimethylacetimidamide

There total 4 articles about (E)-N'-({6-[(diphenylphosphoryl)methyl]pyridin-2-yl}methyl)-N,N-dimethylacetimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 18871-66-4
N,N-dimethylacetamide dimethyl acetal

: 1610436-26-4
{[6-(aminomethyl)pyridin-2-yl]methyl}diphenylphosphine oxide

: 1620658-08-3
(E)-N'-({6-[(diphenylphosphoryl)methyl]pyridin-2-yl}methyl)-N,N-dimethylacetimidamide

Guidance literature:: With dimethyl amine; In tetrahydrofuran; at 23 ℃; for 18.1667h; Inert atmosphere; Schlenk technique; Darkness;
DOI:10.1002/ejoc.201400120

Reference yield:

: 628308-52-1
2-{[6-(chloromethyl)pyridin-2-yl]methyl}isoindoline-1,3-dione

: 1620658-08-3
(E)-N'-({6-[(diphenylphosphoryl)methyl]pyridin-2-yl}methyl)-N,N-dimethylacetimidamide

Guidance literature:: Multi-step reaction with 3 steps

1: 16 h / 120 °C / Inert atmosphere; Schlenk technique

2: hydrazine hydrate / methanol / 16 h / 90 °C / Inert atmosphere; Schlenk technique

3: dimethyl amine / tetrahydrofuran / 18.17 h / 23 °C / Inert atmosphere; Schlenk technique; Darkness

With hydrazine hydrate; dimethyl amine; In tetrahydrofuran; methanol;
DOI:10.1002/ejoc.201400120

Reference yield:

: 1620657-78-4
2-({6-[(diphenylphosphoryl)methyl]pyridin-2-yl}methyl)isoindoline-1,3-dione

: 1620658-08-3
(E)-N'-({6-[(diphenylphosphoryl)methyl]pyridin-2-yl}methyl)-N,N-dimethylacetimidamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 16 h / 90 °C / Inert atmosphere; Schlenk technique

2: dimethyl amine / tetrahydrofuran / 18.17 h / 23 °C / Inert atmosphere; Schlenk technique; Darkness

With hydrazine hydrate; dimethyl amine; In tetrahydrofuran; methanol;
DOI:10.1002/ejoc.201400120