N-{[6-(1,3-dioxolan-2-yl)pyridin-2-yl]methoxy}-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine

Base Information

Chemical Name:N-{[6-(1,3-dioxolan-2-yl)pyridin-2-yl]methoxy}-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine
CAS No.:1187835-33-1
Molecular Formula:C₁₈H₁₈N₆O₃
Molecular Weight:366.379
Hs Code.:

Synonyms:N-{[6-(1,3-dioxolan-2-yl)pyridin-2-yl]methoxy}-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine

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Chemical Property of N-{[6-(1,3-dioxolan-2-yl)pyridin-2-yl]methoxy}-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine

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Technology Process of N-{[6-(1,3-dioxolan-2-yl)pyridin-2-yl]methoxy}-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine

There total 5 articles about N-{[6-(1,3-dioxolan-2-yl)pyridin-2-yl]methoxy}-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: N-hydroxy-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine

: 1187836-96-9
1-{[6-(1,3-dioxolan-2-yl)pyridin-2-yl]methyl}pyridinium bromide hydrobromide

: 1187835-33-1
N-{[6-(1,3-dioxolan-2-yl)pyridin-2-yl]methoxy}-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine

Guidance literature:: With DBN; In acetonitrile; at 0 - 20 ℃;

Reference yield:

: 1122-72-1
6-methyl-2-pyridinecarboxaldehyde

: 1187835-33-1
N-{[6-(1,3-dioxolan-2-yl)pyridin-2-yl]methoxy}-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / 0.05 h / 200 °C / Microwave irradiation

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 - 26 °C

3.1: trifluoroacetic acid / dichloromethane / 2 h

3.2: 2 h

4.1: sulfurous dibromide / dichloromethane / 5 - 20 °C

5.1: DBN / acetonitrile / 0 - 20 °C

With sulfurous dibromide; DBN; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In dichloromethane; acetonitrile;

Reference yield:

: 897943-12-3
2-[1,3]dioxolan-2-yl-6-methylpyridine 1-oxide

: 1187835-33-1
N-{[6-(1,3-dioxolan-2-yl)pyridin-2-yl]methoxy}-1-(1-methyl-1H-tetrazol-5-yl)-1-phenylmethanimine

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 2 h

1.2: 2 h

2.1: sulfurous dibromide / dichloromethane / 5 - 20 °C

3.1: DBN / acetonitrile / 0 - 20 °C

With sulfurous dibromide; DBN; trifluoroacetic acid; In dichloromethane; acetonitrile;