3-phenyl-2-(5,6,7,8-tetraphenylnaphthalen-1-yl)-8,9-dihydro-7H-benzo[de]quinoline

Base Information

Chemical Name:3-phenyl-2-(5,6,7,8-tetraphenylnaphthalen-1-yl)-8,9-dihydro-7H-benzo[de]quinoline
CAS No.:1648787-33-0
Molecular Formula:C₅₂H₃₇N
Molecular Weight:675.872
Hs Code.:

Synonyms:3-phenyl-2-(5,6,7,8-tetraphenylnaphthalen-1-yl)-8,9-dihydro-7H-benzo[de]quinoline

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Chemical Property of 3-phenyl-2-(5,6,7,8-tetraphenylnaphthalen-1-yl)-8,9-dihydro-7H-benzo[de]quinoline

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Technology Process of 3-phenyl-2-(5,6,7,8-tetraphenylnaphthalen-1-yl)-8,9-dihydro-7H-benzo[de]quinoline

There total 2 articles about 3-phenyl-2-(5,6,7,8-tetraphenylnaphthalen-1-yl)-8,9-dihydro-7H-benzo[de]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 104354-39-4,192461-77-1
3,4-dihydro-naphthalen-1(2H)-one oxime O-methyl ether

: 501-65-5
diphenyl acetylene

: 1648787-33-0
3-phenyl-2-(5,6,7,8-tetraphenylnaphthalen-1-yl)-8,9-dihydro-7H-benzo[de]quinoline

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate; sodium acetate; In methanol; at 110 ℃; for 2h; Time; Schlenk technique; Inert atmosphere;
DOI:10.1002/adsc.201400292

Reference yield: 55.0%

: 501-65-5
diphenyl acetylene

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 1648787-33-0
3-phenyl-2-(5,6,7,8-tetraphenylnaphthalen-1-yl)-8,9-dihydro-7H-benzo[de]quinoline

Guidance literature:: diphenyl acetylene; 3,4-dihydronaphthalene-1(2H)-one; With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver(I) acetate; hydroxylamine-O-sulfonic acid; In methanol; at 70 ℃; Schlenk technique; Inert atmosphere;

With copper diacetate; In methanol; at 110 ℃; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.0c02582