C₂₂H₂₂N₂O₃

Base Information

Chemical Name:C₂₂H₂₂N₂O₃
CAS No.:935549-56-7
Molecular Formula:C₂₂H₂₂N₂O₃
Molecular Weight:362.428
Hs Code.:

C<sub>22</sub>H<sub>22</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₂H₂₂N₂O₃

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Chemical Property of C₂₂H₂₂N₂O₃

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Technology Process of C₂₂H₂₂N₂O₃

There total 1 articles about C₂₂H₂₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₁₅NO₂

: 5176-27-2
N-tert-butyloxycarbonyl-pyrrole

: 74087-85-7
3,3-dimethyldioxirane

: 935549-56-7
C₂₂H₂₂N₂O₃

Guidance literature:: C₁₈H₁₅NO₂; N-tert-butyloxycarbonyl-pyrrole; 3,3-dimethyldioxirane; With 4 A molecular sieve; zinc(II) chloride; In diethyl ether; dichloromethane; acetone; at -45 ℃; for 48h;

With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 3h; under 760.051 Torr;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 12h; Further stages.;
DOI:10.1021/ol070103n

Reference yield: 88.0%

: 935549-56-7
C₂₂H₂₂N₂O₃

: 106-95-6
allyl bromide

: 935549-57-8
C₂₅H₂₆N₂O₃

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1021/ol070103n

Reference yield:

: 935549-56-7
C₂₂H₂₂N₂O₃

: C₂₆H₂₆N₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: 88 percent / K₂CO₃ / dimethylformamide / 12 h / 20 °C

2.1: LHMDS; HMPA / tetrahydrofuran / 0.5 h / 0 - 20 °C

2.2: 40 percent / tetrahydrofuran / 12 h / 20 °C

3.1: 36 percent / Grubbs'-G₁ / CH₂Cl₂ / 48 h / 40 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium carbonate; lithium hexamethyldisilazane; Grubbs'-G₁; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol070103n