2,5-epoxy-2-(4-methoxyphenyl)-4-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepin-3-one

Base Information

Chemical Name:2,5-epoxy-2-(4-methoxyphenyl)-4-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepin-3-one
CAS No.:845464-11-1
Molecular Formula:C₂₂H₁₇NO₄
Molecular Weight:359.381
Hs Code.:

Synonyms:2,5-epoxy-2-(4-methoxyphenyl)-4-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepin-3-one

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Chemical Property of 2,5-epoxy-2-(4-methoxyphenyl)-4-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepin-3-one

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Technology Process of 2,5-epoxy-2-(4-methoxyphenyl)-4-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepin-3-one

There total 3 articles about 2,5-epoxy-2-(4-methoxyphenyl)-4-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 650-51-1
sodium trichloroacetate

: 4-Methoxy-benzoic acid 2-[(E)-phenyliminomethyl]-phenyl ester

: 845464-11-1
2,5-epoxy-2-(4-methoxyphenyl)-4-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepin-3-one

Guidance literature:: With N-benzyl-N,N,N-triethylammonium chloride; In chloroform; at 60 ℃; for 1h;
DOI:10.1023/B:RUCB.0000041304.68814.83

Reference yield:

: 479354-30-8
10,10-difluoro-9-(4-methoxy-phenyl)-11-phenyl-8,12-dioxa-11-aza-tricyclo[7.2.1.0^2,7]dodeca-2,4,6-triene

: 845464-11-1
2,5-epoxy-2-(4-methoxyphenyl)-4-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepin-3-one

Guidance literature:: With water; silica gel; In hexane; ethyl acetate;
DOI:10.1039/b204464a

Reference yield:

: 4-Methoxy-benzoic acid 2-[(E)-phenyliminomethyl]-phenyl ester

: 845464-11-1
2,5-epoxy-2-(4-methoxyphenyl)-4-phenyl-2,3,4,5-tetrahydro-1,4-benzoxazepin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / Pb; Bu₄NBr / CH₂Cl₂ / 19 h / 45 °C / ultrasonic irradiation

2: H₂O; silica / hexane; ethyl acetate

With Piperonyl butoxide; tetrabutylammomium bromide; water; silica gel; In hexane; dichloromethane; ethyl acetate;
DOI:10.1039/b204464a