C₃₁H₃₉NO₆Si

Base Information

Chemical Name:C₃₁H₃₉NO₆Si
CAS No.:1267651-85-3
Molecular Formula:C₃₁H₃₉NO₆Si
Molecular Weight:549.739
Hs Code.:

C<sub>31</sub>H<sub>39</sub>NO<sub>6</sub>Si

Synonyms:C₃₁H₃₉NO₆Si

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Chemical Property of C₃₁H₃₉NO₆Si

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Technology Process of C₃₁H₃₉NO₆Si

There total 8 articles about C₃₁H₃₉NO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1267651-84-2
C₃₄H₄₃NO₆Si

: 1267651-85-3
C₃₁H₃₉NO₆Si

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 20 ℃; for 2h;
DOI:10.1021/ol103094j

Reference yield:

: 870137-18-1
(R)-4-((R)-1-hydroxy-1-methylprop-2-ynyl)-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 1267651-85-3
C₃₁H₃₉NO₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

2: 1,4-bis-(9-O-dihydroquinidinyl)phthalazine; methanesulfonamide / water; tert-butyl alcohol / 24 h / 20 °C

3: dmap; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

4: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 12 h / 50 °C / Inert atmosphere

5: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

6: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

With dmap; 1,4-bis-(9-O-dihydroquinidinyl)phthalazine; lithium aluminium tetrahydride; methanesulfonamide; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; tert-butyl alcohol;
DOI:10.1021/ol103094j

Reference yield:

: 1267651-79-5
C₃₀H₄₅NO₆Si

: 1267651-85-3
C₃₁H₃₉NO₆Si

Guidance literature:: Multi-step reaction with 3 steps

1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 12 h / 50 °C / Inert atmosphere

2: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

3: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

With sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; 1,2-dichloro-ethane;
DOI:10.1021/ol103094j