[(3-t-butyldimethylsilyloxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane

Base Information

• Chemical Name: [(3-t-butyldimethylsilyloxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane
• CAS No.: 552848-19-8
• Molecular Formula: C₂₅H₃₇ClO₃Si
• Molecular Weight: 455.058

Synonyms:[(3-t-butyldimethylsilyloxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane

Chemical Property of [(3-t-butyldimethylsilyloxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane

Chemical Property:

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Technology Process of [(3-t-butyldimethylsilyloxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane

There total 1 articles about [(3-t-butyldimethylsilyloxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-methoxy(D3)-2-adamantanone (552848-14-3) + C14H18(2)H3ClO3Si (552847-85-5) → [(3-t-butyldimethylsilyloxy-4-chlorophenyl)-2-methoxy(D3)-methylene]-5-methoxy(D3)adamantane (552848-19-8)

Guidance literature:

With titanium tetrachloride; triethylamine; zinc; In tetrahydrofuran; for 12.8333h; Heating / reflux;

Reference yield:

[(3-t-butyldimethylsilyloxy-4-chlorophenyl)-2-methoxy(D3)-methylene]-5-methoxy(D3)adamantane (552848-19-8) → [(3-hydroxy-4-chlorophenyl)-2-methoxy(D3)-methylene]-5-methoxy(D3)adamantane (552848-20-1)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 1.66667h;

upstream raw materials:

5-methoxy(D₃)-2-adamantanone

C₁₄H₁₈⁽²⁾H₃ClO₃Si

Downstream raw materials:

[(3-hydroxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane

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