2-(3-(4-(tert-butyl)phenyl)-2-methylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(3-(4-(tert-butyl)phenyl)-2-methylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1379610-63-5
Molecular Formula:C₂₀H₃₃BO₂
Molecular Weight:316.292
Hs Code.:

Synonyms:2-(3-(4-(tert-butyl)phenyl)-2-methylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-(3-(4-(tert-butyl)phenyl)-2-methylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(3-(4-(tert-butyl)phenyl)-2-methylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 3 articles about 2-(3-(4-(tert-butyl)phenyl)-2-methylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1367368-43-1
C₂₁H₂₈N₂O₂S

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1379610-63-5
2-(3-(4-(tert-butyl)phenyl)-2-methylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: C₂₁H₂₈N₂O₂S; With sodium methylate; benzyltrimethylammonium chloride; In toluene; at 20 ℃; for 1h; Inert atmosphere;

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In toluene; at 90 ℃; Inert atmosphere;
DOI:10.1002/anie.201108139

Reference yield: 60.0%

: (CH₃)3CC₆H₄CH₂CH(CH₃)CH(N₂SO₂C₆H₄CH₃)^(1-)*Na⁽¹⁺⁾=Na(CH₃)3CC₆H₄CH₂CH(CH₃)CH(N₂SO₂C₆H₄CH₃)

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1379610-63-5
2-(3-(4-(tert-butyl)phenyl)-2-methylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With Me₃BzNCl; 90°C, 1-24 h;
DOI:10.1002/anie.201108139

Reference yield:

: 80-54-6
lilial

: 1379610-63-5
2-(3-(4-(tert-butyl)phenyl)-2-methylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 70 °C / Inert atmosphere

2.1: sodium methylate; benzyltrimethylammonium chloride / toluene / 1 h / 20 °C / Inert atmosphere

2.2: 90 °C / Inert atmosphere

With sodium methylate; benzyltrimethylammonium chloride; In methanol; toluene;
DOI:10.1002/anie.201108139