8-(5-(3,4-dichlorophenyl)-1H-pyrazol-3-yl)-1,4-dioxa-8-azaspiro[4.5]decane

Base Information

Chemical Name:8-(5-(3,4-dichlorophenyl)-1H-pyrazol-3-yl)-1,4-dioxa-8-azaspiro[4.5]decane
CAS No.:1088709-92-5
Molecular Formula:C₁₆H₁₇Cl₂N₃O₂
Molecular Weight:354.236
Hs Code.:

Synonyms:8-(5-(3,4-dichlorophenyl)-1H-pyrazol-3-yl)-1,4-dioxa-8-azaspiro[4.5]decane

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Chemical Property of 8-(5-(3,4-dichlorophenyl)-1H-pyrazol-3-yl)-1,4-dioxa-8-azaspiro[4.5]decane

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Technology Process of 8-(5-(3,4-dichlorophenyl)-1H-pyrazol-3-yl)-1,4-dioxa-8-azaspiro[4.5]decane

There total 1 articles about 8-(5-(3,4-dichlorophenyl)-1H-pyrazol-3-yl)-1,4-dioxa-8-azaspiro[4.5]decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56944-70-8
3,4-dichlorophenyl α-oxoketen dithioacetal

: 177-11-7
4,4-ethylenedioxy-piperidine

: 1088709-92-5
8-(5-(3,4-dichlorophenyl)-1H-pyrazol-3-yl)-1,4-dioxa-8-azaspiro[4.5]decane

Guidance literature:: 3,4-dichlorophenyl α-oxoketen dithioacetal; 4,4-ethylenedioxy-piperidine; In ethanol; at 80 ℃;

With hydrazine; In ethanol; at 80 ℃;

Reference yield:

: 1088709-92-5
8-(5-(3,4-dichlorophenyl)-1H-pyrazol-3-yl)-1,4-dioxa-8-azaspiro[4.5]decane

: 1088708-97-7
C₂₀H₂₇Cl₂N₅

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / 1,4-dioxane / 2 h / 50 °C

2: sodium tris(acetoxy)borohydride; acetic acid / tetrahydrofuran / pH 4 - 5

With hydrogenchloride; water; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; 1,4-dioxane;