C₄₁H₃₅BrN₈O₆S₂

Base Information

Chemical Name:C₄₁H₃₅BrN₈O₆S₂
CAS No.:1333378-11-2
Molecular Formula:C₄₁H₃₅BrN₈O₆S₂
Molecular Weight:879.815
Hs Code.:

C<sub>41</sub>H<sub>35</sub>BrN<sub>8</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₄₁H₃₅BrN₈O₆S₂

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Chemical Property of C₄₁H₃₅BrN₈O₆S₂

Chemical Property:

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Technology Process of C₄₁H₃₅BrN₈O₆S₂

There total 19 articles about C₄₁H₃₅BrN₈O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1333378-12-3
C₃₁H₃₁N₇O₄S₂

: 108061-76-3
2-(6-bromo-1H-indol-3-yl)-2-oxoacetyl chloride

: 1333378-11-2
C₄₁H₃₅BrN₈O₆S₂

Guidance literature:: With dmap; triethylamine; In toluene; at 0 - 40 ℃;
DOI:10.1002/ejoc.201100242

Reference yield:

: C₁₃H₁₅BrN₂O₃

: 1333378-11-2
C₄₁H₃₅BrN₈O₆S₂

Guidance literature:: Multi-step reaction with 14 steps

1: acetic acid; zinc / water / 1.83 h / 80 - 85 °C

2: glyoxylic acid ethyl ester; magnesium sulfate / dichloromethane / 0 - 20 °C

3: dmap; triethylamine / toluene / 18 h / 70 °C

4: ammonium cerium (IV) nitrate / water; acetonitrile / 0.25 h / -15 °C

5: dichloromethane / 4 h / 20 °C

6: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 1,4-dioxane / 21 h / 100 °C

7: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.33 h / 0 °C

8: hydrogen bromide; acetic acid / tetrahydrofuran / 0.5 h / 0 °C

9: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium ethanolate; caesium carbonate / 1,4-dioxane / 4 h / 100 °C

10: lithium borohydride / tetrahydrofuran / 0 - 20 °C

11: dmap; triethylamine / dichloromethane / 10 h / 20 °C

12: sodium azide / N,N-dimethyl-formamide / 4 h / 80 °C

13: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

14: dmap; triethylamine / toluene / 0 - 40 °C

With dmap; copper(l) iodide; lithium borohydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; glyoxylic acid ethyl ester; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; hydrogen bromide; sodium ethanolate; magnesium sulfate; caesium carbonate; acetic acid; triethylamine; trifluoroacetic acid; zinc; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 6: Sonogashira coupling / 9: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1002/ejoc.201100242

Reference yield:

: 1094172-65-2
C₂₀H₂₁BrN₂O₄

: 1333378-11-2
C₄₁H₃₅BrN₈O₆S₂

Guidance literature:: Multi-step reaction with 12 steps

1: dmap; triethylamine / toluene / 18 h / 70 °C

2: ammonium cerium (IV) nitrate / water; acetonitrile / 0.25 h / -15 °C

3: dichloromethane / 4 h / 20 °C

4: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 1,4-dioxane / 21 h / 100 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.33 h / 0 °C

6: hydrogen bromide; acetic acid / tetrahydrofuran / 0.5 h / 0 °C

7: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium ethanolate; caesium carbonate / 1,4-dioxane / 4 h / 100 °C

8: lithium borohydride / tetrahydrofuran / 0 - 20 °C

9: dmap; triethylamine / dichloromethane / 10 h / 20 °C

10: sodium azide / N,N-dimethyl-formamide / 4 h / 80 °C

11: trifluoroacetic acid / dichloromethane / 2 h / 0 °C

12: dmap; triethylamine / toluene / 0 - 40 °C

With dmap; copper(l) iodide; lithium borohydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; hydrogen bromide; sodium ethanolate; caesium carbonate; acetic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 4: Sonogashira coupling / 7: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1002/ejoc.201100242