(S)-4-(3-(1H-phenanthro[9,10-d]imidazol-2-yl)-1H-indol-1-yl)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)butan-2-ol

Base Information

Chemical Name:(S)-4-(3-(1H-phenanthro[9,10-d]imidazol-2-yl)-1H-indol-1-yl)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)butan-2-ol
CAS No.:1356140-18-5
Molecular Formula:C₄₈H₄₁N₃O₄
Molecular Weight:723.871
Hs Code.:

Synonyms:(S)-4-(3-(1H-phenanthro[9,10-d]imidazol-2-yl)-1H-indol-1-yl)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)butan-2-ol

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Chemical Property of (S)-4-(3-(1H-phenanthro[9,10-d]imidazol-2-yl)-1H-indol-1-yl)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)butan-2-ol

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Technology Process of (S)-4-(3-(1H-phenanthro[9,10-d]imidazol-2-yl)-1H-indol-1-yl)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)butan-2-ol

There total 4 articles about (S)-4-(3-(1H-phenanthro[9,10-d]imidazol-2-yl)-1H-indol-1-yl)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1356140-16-3
(S)-4-(3-(1H-phenanthro[9,10-d]imidazol-2-yl)-1H-indol-1-yl)butane-1,2-diol

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1356140-18-5
(S)-4-(3-(1H-phenanthro[9,10-d]imidazol-2-yl)-1H-indol-1-yl)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)butan-2-ol

Guidance literature:: With pyridine; ammonia; at 20 ℃; for 72h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.11.013

Reference yield:

: C₁₆H₁₉NO₃

: 1356140-18-5
(S)-4-(3-(1H-phenanthro[9,10-d]imidazol-2-yl)-1H-indol-1-yl)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)butan-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / water; N,N-dimethyl-formamide; mineral oil / 2 h / 20 °C / Inert atmosphere

2.1: ammonium acetate / 72 h / 90 °C

2.2: pH 7

3.1: methanol; ammonia / 72 h / 20 °C

4.1: pyridine; ammonia / 72 h / 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; methanol; ammonium acetate; ammonia; In water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.bmc.2011.11.013

Reference yield:

: 1356140-12-9
(S)-1-(3,4-dihydroxybutyl)-1H-indole-3-carbaldehyde

: 1356140-18-5
(S)-4-(3-(1H-phenanthro[9,10-d]imidazol-2-yl)-1H-indol-1-yl)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)butan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium acetate / 72 h / 90 °C

1.2: pH 7

2.1: methanol; ammonia / 72 h / 20 °C

3.1: pyridine; ammonia / 72 h / 20 °C / Inert atmosphere

With pyridine; methanol; ammonium acetate; ammonia;
DOI:10.1016/j.bmc.2011.11.013