3-<4-(5-methyl-4-phenyl-1H-imidazol-1-yl)-1-butenyl>-2-nitro-N,N-dimethylaniline

Base Information

Chemical Name:3-<4-(5-methyl-4-phenyl-1H-imidazol-1-yl)-1-butenyl>-2-nitro-N,N-dimethylaniline
CAS No.:149155-81-7
Molecular Formula:C₂₂H₂₄N₄O₂
Molecular Weight:376.458
Hs Code.:

Synonyms:3-<4-(5-methyl-4-phenyl-1H-imidazol-1-yl)-1-butenyl>-2-nitro-N,N-dimethylaniline

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Chemical Property of 3-<4-(5-methyl-4-phenyl-1H-imidazol-1-yl)-1-butenyl>-2-nitro-N,N-dimethylaniline

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Technology Process of 3-<4-(5-methyl-4-phenyl-1H-imidazol-1-yl)-1-butenyl>-2-nitro-N,N-dimethylaniline

There total 7 articles about 3-<4-(5-methyl-4-phenyl-1H-imidazol-1-yl)-1-butenyl>-2-nitro-N,N-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 149155-88-4
3-(5-methyl-4-phenyl-1H-imidazol-1-yl)propionaldehyde

: <3-(dimethylamino)-2-nitrobenzyl>triphenylphosphonium bromide

: 149155-81-7
3-<4-(5-methyl-4-phenyl-1H-imidazol-1-yl)-1-butenyl>-2-nitro-N,N-dimethylaniline

Guidance literature:: With sodium ethanolate; In ethanol; for 2h; Heating;
DOI:10.1021/jm00063a013

Reference yield:

: 4771-47-5
3-chloro-2-nitro-benzoic acid

: 149155-81-7
3-<4-(5-methyl-4-phenyl-1H-imidazol-1-yl)-1-butenyl>-2-nitro-N,N-dimethylaniline

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / B₂H₆ / tetrahydrofuran / 2 h / Ambient temperature

2: 76 percent / H₂O; dimethylformamide / 4 h / 120 °C

3: 49 percent / PBr₃ / dimethylformamide / 1 h / Ambient temperature

4: 96 percent / toluene / 1 h / Heating

5: 63 percent / EtONa / ethanol / 2 h / Heating

With sodium ethanolate; phosphorus tribromide; diborane; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00063a013

Reference yield:

: 77158-86-2
(3-chloro-2-nitrophenyl)methanol

: 149155-81-7
3-<4-(5-methyl-4-phenyl-1H-imidazol-1-yl)-1-butenyl>-2-nitro-N,N-dimethylaniline

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / H₂O; dimethylformamide / 4 h / 120 °C

2: 49 percent / PBr₃ / dimethylformamide / 1 h / Ambient temperature

3: 96 percent / toluene / 1 h / Heating

4: 63 percent / EtONa / ethanol / 2 h / Heating

With sodium ethanolate; phosphorus tribromide; In ethanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00063a013