{(5S)-5-[(R)-2-(methoxymethoxy)pent-4-enyl]-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl}methanol

Base Information

• Chemical Name: {(5S)-5-[(R)-2-(methoxymethoxy)pent-4-enyl]-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl}methanol
• CAS No.: 1198463-63-6
• Molecular Formula: C₁₈H₂₆O₆
• Molecular Weight: 338.401

Synonyms:{(5S)-5-[(R)-2-(methoxymethoxy)pent-4-enyl]-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl}methanol

Chemical Property of {(5S)-5-[(R)-2-(methoxymethoxy)pent-4-enyl]-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl}methanol

Chemical Property:

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Technology Process of {(5S)-5-[(R)-2-(methoxymethoxy)pent-4-enyl]-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl}methanol

There total 3 articles about {(5S)-5-[(R)-2-(methoxymethoxy)pent-4-enyl]-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl}methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C24H31NO6 → {(5R)-5-[(R)-2-(methoxymethoxy)pent-4-enyl]-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl}methanol + {(5S)-5-[(R)-2-(methoxymethoxy)pent-4-enyl]-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl}methanol (1198463-63-6)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; at 0 - 20 ℃; optical yield given as %de; Inert atmosphere;

DOI:10.1021/ja907924j

Reference yield:

C24H31NO6 → {(5S)-5-[(R)-2-(methoxymethoxy)pent-4-enyl]-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl}methanol (1198463-63-6) + {5-[(R)-2-(methoxymethoxy)pent-4-enyl]-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl}methanol

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; at 0 - 20 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;

DOI:10.1002/chem.201102898

Reference yield:

(5R)-1-(2-ethyl-1H-pyrrol-1-yl)-2,3-dihydroxy-5-(methoxymethoxy)oct-7-en-1-one → {(5S)-5-[(R)-2-(methoxymethoxy)pent-4-enyl]-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl}methanol (1198463-63-6) + {5-[(R)-2-(methoxymethoxy)pent-4-enyl]-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl}methanol

Guidance literature:

Multi-step reaction with 2 steps

1: camphor-10-sulfonic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; camphor-10-sulfonic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1002/chem.201102898

Downstream raw materials:

C₁₈H₂₄O₆

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