bromo((2,6-dichlorophenoxy)dimethylgermyl)bis(trimethylsilyl)methane

Base Information

Chemical Name:bromo((2,6-dichlorophenoxy)dimethylgermyl)bis(trimethylsilyl)methane
CAS No.:103349-24-2
Molecular Formula:C₁₅H₂₇BrCl₂GeOSi₂
Molecular Weight:502.95
Hs Code.:

Synonyms:bromo((2,6-dichlorophenoxy)dimethylgermyl)bis(trimethylsilyl)methane

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Chemical Property of bromo((2,6-dichlorophenoxy)dimethylgermyl)bis(trimethylsilyl)methane

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Technology Process of bromo((2,6-dichlorophenoxy)dimethylgermyl)bis(trimethylsilyl)methane

There total 1 articles about bromo((2,6-dichlorophenoxy)dimethylgermyl)bis(trimethylsilyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 87-65-0
2,6-Dichlorophenol

: 103349-20-8
Ge(CH₃)2BrCBr[Si(CH₃)3]2

: 103349-24-2
bromo((2,6-dichlorophenoxy)dimethylgermyl)bis(trimethylsilyl)methane

Guidance literature:: With N(C₂H₅)(CH₃)2; In pentane; byproducts: (CH3)2(C2H5)NHBr; exclusion of air and water; 4 h at room temperature; filtration; removal of solvent in high vac. at room temperature; fractionated distn. in high vac. at 50°C; elem. anal.;

Reference yield: 100.0%

: 103349-24-2
bromo((2,6-dichlorophenoxy)dimethylgermyl)bis(trimethylsilyl)methane

: 103349-32-2
(dimethylphenoxygermyl)bis(trimethylsilyl)methane

Guidance literature:: With n-butyllithium; phenol; In diethyl ether; exclusion of air and water; dropwise addn. of BuLi (Et2O) at -78°C; addn. of PhOH after 1 h; fractionated high vac. distn. at 60°C; elem. anal.;

Reference yield:

: 103349-24-2
bromo((2,6-dichlorophenoxy)dimethylgermyl)bis(trimethylsilyl)methane

: 103349-38-8
[(dimethylphenoxygermyl)bis(trimethylsilyl)methyl]lithium

Guidance literature:: With n-butyllithium; In diethyl ether; byproducts: butylbromide; exclusion of air and water; dropwise addn. of BuLi (Et2O) at -78°C; warming up to 0°C; evapn. in high vac.;