2-[(1S,6S)-3-(acetoxymethyl)-6-(1-methylethenyl)-2-cyclohexen-1-yl]-5-pentylresorcinol

Base Information

Chemical Name:2-[(1S,6S)-3-(acetoxymethyl)-6-(1-methylethenyl)-2-cyclohexen-1-yl]-5-pentylresorcinol
CAS No.:1605280-36-1
Molecular Formula:C₂₃H₃₂O₄
Molecular Weight:372.505
Hs Code.:

Synonyms:2-[(1S,6S)-3-(acetoxymethyl)-6-(1-methylethenyl)-2-cyclohexen-1-yl]-5-pentylresorcinol

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Chemical Property of 2-[(1S,6S)-3-(acetoxymethyl)-6-(1-methylethenyl)-2-cyclohexen-1-yl]-5-pentylresorcinol

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Technology Process of 2-[(1S,6S)-3-(acetoxymethyl)-6-(1-methylethenyl)-2-cyclohexen-1-yl]-5-pentylresorcinol

There total 7 articles about 2-[(1S,6S)-3-(acetoxymethyl)-6-(1-methylethenyl)-2-cyclohexen-1-yl]-5-pentylresorcinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 1605281-10-4,936001-98-8
[(1S,4S)-1-hydroxy-4-(prop-1-en-2-yl)cyclohex-2-enyl]methyl acetate

: 500-66-3
Olivetol

: 1605280-36-1
2-[(1S,6S)-3-(acetoxymethyl)-6-(1-methylethenyl)-2-cyclohexen-1-yl]-5-pentylresorcinol

Guidance literature:: With toluene-4-sulfonic acid; In benzene; at 0 - 20 ℃; for 4h; Inert atmosphere;

Reference yield:

: 536-59-4,18457-55-1
(-)-perillyl alcohol

: 1605280-36-1
2-[(1S,6S)-3-(acetoxymethyl)-6-(1-methylethenyl)-2-cyclohexen-1-yl]-5-pentylresorcinol

Guidance literature:: Multi-step reaction with 7 steps

1.1: bis(acetylacetonate)oxovanadium; tert.-butylhydroperoxide / toluene; tert-butyl alcohol / 20 °C / Cooling with ice

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0.17 h

2.2: 14 h

3.1: sodium tetrahydroborate / ethanol / 1 h / 20 °C

3.2: 65 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 25 °C / Inert atmosphere

5.1: pyridine / 20 °C / Cooling with ice; Inert atmosphere

6.1: dihydrogen peroxide / tetrahydrofuran; pyridine / 65 °C / Cooling with ice

7.1: toluene-4-sulfonic acid / benzene / 4 h / 0 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; tert.-butylhydroperoxide; sodium tetrahydroborate; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; dihydrogen peroxide; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; ethanol; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; benzene;

Reference yield:

: 190718-78-6
((4S)-4-(prop-1-en-2-yl)-7-oxabicyclo[4.1.0]heptan-1-yl)methanol

: 1605280-36-1
2-[(1S,6S)-3-(acetoxymethyl)-6-(1-methylethenyl)-2-cyclohexen-1-yl]-5-pentylresorcinol

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 0.17 h

1.2: 14 h

2.1: sodium tetrahydroborate / ethanol / 1 h / 20 °C

2.2: 65 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 25 °C / Inert atmosphere

4.1: pyridine / 20 °C / Cooling with ice; Inert atmosphere

5.1: dihydrogen peroxide / tetrahydrofuran; pyridine / 65 °C / Cooling with ice

6.1: toluene-4-sulfonic acid / benzene / 4 h / 0 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; sodium tetrahydroborate; tetrabutyl ammonium fluoride; dihydrogen peroxide; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; ethanol; N,N-dimethyl-formamide; benzene;