(14S,17S,18S,20S)-N-((3S,11bR)-9,11-bis(benzyloxy)-2,3,4,6,7,11b-hexahydro-4-oxo-1H-pyrido[2,1-a]isoquinolin-3-yl)-14,17,18-trihydroxy-20-methyloctacosanamide

Base Information

Chemical Name:(14S,17S,18S,20S)-N-((3S,11bR)-9,11-bis(benzyloxy)-2,3,4,6,7,11b-hexahydro-4-oxo-1H-pyrido[2,1-a]isoquinolin-3-yl)-14,17,18-trihydroxy-20-methyloctacosanamide
CAS No.:1147745-25-2
Molecular Formula:C₅₆H₈₄N₂O₇
Molecular Weight:897.292
Hs Code.:

(14S,17S,18S,20S)-N-((3S,11bR)-9,11-bis(benzyloxy)-2,3,4,6,7,11b-hexahydro-4-oxo-1H-pyrido[2,1-a]isoquinolin-3-yl)-14,17,18-trihydroxy-20-methyloctacosanamide

Synonyms:(14S,17S,18S,20S)-N-((3S,11bR)-9,11-bis(benzyloxy)-2,3,4,6,7,11b-hexahydro-4-oxo-1H-pyrido[2,1-a]isoquinolin-3-yl)-14,17,18-trihydroxy-20-methyloctacosanamide

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Chemical Property of (14S,17S,18S,20S)-N-((3S,11bR)-9,11-bis(benzyloxy)-2,3,4,6,7,11b-hexahydro-4-oxo-1H-pyrido[2,1-a]isoquinolin-3-yl)-14,17,18-trihydroxy-20-methyloctacosanamide

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Technology Process of (14S,17S,18S,20S)-N-((3S,11bR)-9,11-bis(benzyloxy)-2,3,4,6,7,11b-hexahydro-4-oxo-1H-pyrido[2,1-a]isoquinolin-3-yl)-14,17,18-trihydroxy-20-methyloctacosanamide

There total 1 articles about (14S,17S,18S,20S)-N-((3S,11bR)-9,11-bis(benzyloxy)-2,3,4,6,7,11b-hexahydro-4-oxo-1H-pyrido[2,1-a]isoquinolin-3-yl)-14,17,18-trihydroxy-20-methyloctacosanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1147745-22-9
(E,14S,20S)-N-((3S,11bR)-9,11-bis(benzyloxy)-2,3,4,6,7,11b-hexahydro-4-oxo-1H-pyrido[2,1-a]isoquinolin-3-yl)-14-hydroxy-20-methyloctacos-17-enamide

: 1147745-25-2
(14S,17S,18S,20S)-N-((3S,11bR)-9,11-bis(benzyloxy)-2,3,4,6,7,11b-hexahydro-4-oxo-1H-pyrido[2,1-a]isoquinolin-3-yl)-14,17,18-trihydroxy-20-methyloctacosanamide

: (14S,17R,18R,20S)-N-((3S,11bR)-9,11-bis(benzyloxy)-2,3,4,6,7,11b-hexahydro-4-oxo-1H-pyrido[2,1-a]isoquinolin-3-yl)-14,17,18-trihydroxy-20-methyloctacosanamide

Guidance literature:: With methanesulfonamide; AD-mix α; water; In tetrahydrofuran; tert-butyl methyl ether; tert-butyl alcohol; at 0 ℃; for 18h; optical yield given as %de;